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使用具有可编程尺寸的纳米制造校准样品定量扫描热显微镜的探针-样品相互作用。

Quantification of probe-sample interactions of a scanning thermal microscope using a nanofabricated calibration sample having programmable size.

机构信息

School of Engineering, University of Glasgow, Rankine Building, Oakfield Avenue, Glasgow G12 8LT, UK.

出版信息

Nanotechnology. 2016 Aug 12;27(32):325503. doi: 10.1088/0957-4484/27/32/325503. Epub 2016 Jul 1.

Abstract

We report a method for quantifying scanning thermal microscopy (SThM) probe-sample thermal interactions in air using a novel temperature calibration device. This new device has been designed, fabricated and characterised using SThM to provide an accurate and spatially variable temperature distribution that can be used as a temperature reference due to its unique design. The device was characterised by means of a microfabricated SThM probe operating in passive mode. This data was interpreted using a heat transfer model, built to describe the thermal interactions during a SThM thermal scan. This permitted the thermal contact resistance between the SThM tip and the device to be determined as 8.33 × 10(5) K W(-1). It also permitted the probe-sample contact radius to be clarified as being the same size as the probe's tip radius of curvature. Finally, the data were used in the construction of a lumped-system steady state model for the SThM probe and its potential applications were addressed.

摘要

我们报告了一种在空气中使用新型温度校准装置量化扫描热显微镜 (SThM) 探针-样品热相互作用的方法。该新型装置采用 SThM 设计、制造和特性化,由于其独特的设计,提供了一个准确且空间变化的温度分布,可用作温度参考。该装置通过在无源模式下运行的微制造 SThM 探针进行了表征。使用传热模型对该数据进行了解释,该模型用于描述 SThM 热扫描期间的热相互作用。这使得能够确定 SThM 尖端和装置之间的热接触电阻为 8.33 × 10(5) K W(-1)。它还澄清了探针-样品接触半径与探针的曲率半径相同。最后,使用该数据构建了 SThM 探针的集中系统稳态模型,并讨论了其潜在应用。

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