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Fabrication of Uniform Nanoporous Oxide Layers on Long Cylindrical Zircaloy Tubes by Anodization Using Multi-Counter Electrodes.

作者信息

Park Yang Jeong, Kim Jung Woo, Ali Ghafar, Kim Hyun Jin, Addad Yacine, Cho Sung Oh

机构信息

Department of Nuclear and Quantum Engineering, Korea Advanced Institute of Science and Technology, 373-1 Guseong, Yuseong, Daejeon, 305-701, Republic of Korea.

Nanomaterials Research Group (NRG), Physics Division (PD), PINSTECH, Islamabad, 45650, Pakistan.

出版信息

Nanoscale Res Lett. 2017 Dec;12(1):20. doi: 10.1186/s11671-016-1774-1. Epub 2017 Jan 6.

DOI:10.1186/s11671-016-1774-1
PMID:28058652
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC5216014/
Abstract

We have presented a method to prepare a uniform anodic nanoporous oxide film on the surface of a cylindrical zircaloy (Zr) tube. The distribution of the electric field around the Zr tube determines the distribution of the thickness of the anodic nanoporous oxide film. The electric field generated when a cylindrical Zr tube is electrochemically anodized was simulated by using commercial code COMSOL. When four Pt wires were used as counter electrodes, a uniform electric field was achieved with minimal use of Pt. Based on the simulation results, a cylindrical Zr tube was anodized and the distribution of the thickness of the anodic nanoporous oxide layer was measured by FESEM. Also, mass production of uniform nanoporous anodic oxide films was possible by symmetrically arranging the zircaloy tubes and Pt wires.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/b3559c2d651f/11671_2016_1774_Fig6_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/fe151a94363a/11671_2016_1774_Fig1_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/4c3a9bfa6b90/11671_2016_1774_Fig2_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/090b55c33102/11671_2016_1774_Fig3_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/7ca2ac52b5fd/11671_2016_1774_Fig4_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/6927ba255652/11671_2016_1774_Fig5_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/b3559c2d651f/11671_2016_1774_Fig6_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/fe151a94363a/11671_2016_1774_Fig1_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/4c3a9bfa6b90/11671_2016_1774_Fig2_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/090b55c33102/11671_2016_1774_Fig3_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/7ca2ac52b5fd/11671_2016_1774_Fig4_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/6927ba255652/11671_2016_1774_Fig5_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d9d2/5216014/b3559c2d651f/11671_2016_1774_Fig6_HTML.jpg

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本文引用的文献

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2
AAO-assisted synthesis of highly ordered, large-scale TiO2 nanowire arrays via sputtering and atomic layer deposition.通过溅射和原子层沉积利用阳极氧化铝辅助合成高度有序的大规模二氧化钛纳米线阵列。
Nanoscale Res Lett. 2015 Apr 8;10:166. doi: 10.1186/s11671-015-0872-9. eCollection 2015.
3
Isotopic evidence of plutonium release into the environment from the Fukushima DNPP accident.
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Sci Rep. 2012;2:304. doi: 10.1038/srep00304. Epub 2012 Mar 8.
4
TiO2 nanotubes: synthesis and applications.TiO2 纳米管：合成与应用。
Angew Chem Int Ed Engl. 2011 Mar 21;50(13):2904-39. doi: 10.1002/anie.201001374. Epub 2011 Mar 10.
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The role of viscous flow of oxide in the growth of self-ordered porous anodic alumina films.氧化物粘性流动在自有序多孔阳极氧化铝膜生长中的作用。
Nat Mater. 2009 May;8(5):415-20. doi: 10.1038/nmat2423. Epub 2009 Apr 12.
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Self-organization of anodic nanotubes on two size scales.
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