Rohr Nadja, Fischer Jens
Division of Dental Materials and Engineering, Department of Reconstructive Dentistry and Temporomandibular Disorders, University Center for Dental Medicine, University of Basel, Switzerland.
J Adv Prosthodont. 2017 Apr;9(2):85-92. doi: 10.4047/jap.2017.9.2.85. Epub 2017 Apr 6.
The aim of this study was to evaluate the effect of tooth surface pre-treatment steps on shear bond strength, which is essential for understanding the adhesive cementation process.
Shear bond strengths of different cements with various tooth surface treatments (none, etching, priming, or etching and priming) on enamel and dentin of human teeth were measured using the Swiss shear test design. Three adhesives (Permaflo DC, Panavia F 2.0, and Panavia V5) and one self-adhesive cement (Panavia SA plus) were included in this study. The interface of the cement and the tooth surface with the different pre-treatments was analyzed using SEM. pH values of the cements and primers were measured.
The highest bond strength values for all cements were achieved with etching and primer on enamel (25.6 ± 5.3 - 32.3 ± 10.4 MPa). On dentin, etching and priming produced the highest bond strength values for all cements (8.6 ± 2.9 - 11.7 ± 3.5 MPa) except for Panavia V5, which achieved significantly higher bond strengths when pre-treated with primer only (15.3 ± 4.1 MPa). Shear bond strength values were correlated with the micro-retentive surface topography of enamel and the tag length on dentin except for Panavia V5, which revealed the highest bond strength with primer application only without etching, resulting in short but sturdy tags.
The highest bond strength can be achieved for Panavia F 2.0, Permaflo DC, and Panavia SA plus when the tooth substrate is previously etched and the respective primer is applied. The new cement Panavia V5 displayed low technique-sensitivity and attained significantly higher adhesion of all tested cements to dentin when only primer was applied.
本研究旨在评估牙齿表面预处理步骤对剪切粘结强度的影响,这对于理解粘结固位过程至关重要。
采用瑞士剪切试验设计,测量不同粘结剂在人牙釉质和牙本质上经过各种牙齿表面处理(无处理、酸蚀、涂底胶或酸蚀加涂底胶)后的剪切粘结强度。本研究纳入了三种粘结剂(Permaflo DC、Panavia F 2.0和Panavia V5)和一种自粘结粘结剂(Panavia SA plus)。使用扫描电子显微镜分析不同预处理条件下粘结剂与牙齿表面的界面。测量粘结剂和底胶的pH值。
所有粘结剂在釉质上酸蚀加涂底胶时获得最高粘结强度值(25.6±5.3 - 32.3±10.4 MPa)。在牙本质上,除Panavia V5外,酸蚀加涂底胶使所有粘结剂获得最高粘结强度值(8.6±2.9 - 11.7±3.5 MPa),Panavia V5仅涂底胶预处理时获得显著更高的粘结强度(15.3±4.1 MPa)。除Panavia V5外,剪切粘结强度值与釉质的微固位表面形貌和牙本质上的标签长度相关,Panavia V5仅涂底胶而不酸蚀时获得最高粘结强度,形成短而牢固的标签。
对于Panavia F 2.0、Permaflo DC和Panavia SA plus,当牙齿基质预先酸蚀并应用相应底胶时可获得最高粘结强度。新型粘结剂Panavia V5显示出低技术敏感性,仅涂底胶时所有测试粘结剂与牙本质的粘结力显著更高。