Henrique Borges Alvaro, Aguirre Guedes Orlando, Evaristo Ricci Volpato Luiz, Siebert Filho Gilberto, Meireles Borba Alexandre, Zina Omar, Piva Evandro, Estrela Carlos
Department of Endodontics, University of Cuiaba, Brazil.
Department of Endodontics, Federal University of Goiás, Brazil.
Iran Endod J. 2017 Summer;12(3):312-317. doi: 10.22037/iej.v12i3.10635.
The aim of this study was to determine the liquid-powder ratio, setting time, solubility, dimensional change, pH, and radiopacity of white structural and non-structural Portland cement, ProRoot MTA and MTA Bio, associated with a 2% glycolic solution containing Aloe Vera, as vehicle.
Five samples of each material were used for each test, according to the American National Standards Institute/American Dental Association (ANSI/ADA) specification No. 57. Statistical analyses were performed using ANOVA and Tukey's test at 5% significance. When sample distribution was not normal, non-parametric analysis of variance and the Kruskal-Wallis test were used (=0.05).
No statistical differences were found in liquid-powder ratios among the tested materials. ProRoot MTA showed the longest setting time. Dimensional change values were acceptable in all groups. Also, no significant differences were found in pH values and pH was alkaline in all samples throughout the experiment. Mean radiopacity results obtained for white Portland cements did not meet ANSI/ADA requirements, and were significantly lower than those obtained for MTA-based cements. Finally, Portland cements showed significantly higher mean solubility values compared to the other samples.
The physicochemical properties of the tested materials in association with Aloe Vera were compatible with ANSI/ADA requirements, except for the white Portland cements, which failed to meet the radiopacity specification.
本研究的目的是测定白色结构型和非结构型波特兰水泥、ProRoot MTA和MTA Bio与含有芦荟的2%乙醇酸溶液作为载体时的液粉比、凝固时间、溶解度、尺寸变化、pH值和射线不透性。
根据美国国家标准学会/美国牙科协会(ANSI/ADA)第57号规范,每种材料取五个样本用于每项测试。采用方差分析和Tukey检验进行统计分析,显著性水平为5%。当样本分布不呈正态时,使用非参数方差分析和Kruskal-Wallis检验(=0.05)。
测试材料之间的液粉比未发现统计学差异。ProRoot MTA的凝固时间最长。所有组的尺寸变化值均可接受。此外,pH值在整个实验过程中均未发现显著差异,且所有样本的pH值均呈碱性。白色波特兰水泥的平均射线不透性结果未达到ANSI/ADA要求,且显著低于基于MTA的水泥。最后,波特兰水泥的平均溶解度值显著高于其他样本。
除白色波特兰水泥未达到射线不透性规范外,测试材料与芦荟相关的物理化学性质符合ANSI/ADA要求。