Department of Operative Dentistry and Periodontology, University Hospital, Ludwig-Maximilians-Universität München, Goethestr. 70, 80336, Munich, Germany.
Clin Oral Investig. 2019 Feb;23(2):747-755. doi: 10.1007/s00784-018-2482-2. Epub 2018 May 18.
The study aims analyzing if improved opacity in modern high-viscosity bulk-fill resin composites (BF-RBC) contradicts with the sufficiency of curing and to assess material's tolerance to less ideal curing conditions.
Simulated large cavities (10 × 6) mm were filled in one increment with three BF-RBCs (Filtek One, FO; Tetric Evo Ceram Bulk Fill, TEC-BF; SonicFill2, SF2). One central and two peripheral (4 mm apart from the center) micromechanical property line-profiles (HV, Vickers hardness; Y, indentation modulus) were measured in 0.2-mm steps at 24 h post-polymerization (n = 6). Depth of cure (DOC) was calculated from the HV variation in depth. A scratch test (DOC) estimated the tolerance in polymerization when simulating clinically relevant curing conditions (exposure distance up to 7 mm; centered and with a 3-mm offset placement of the LCU). Irradiance and spectral distribution of the used light curing unit (LCU) were assessed at various curing conditions.
DOC varied among 3.6 mm (SF2, peripheral) and 5.7 mm (FO, central). The BF-RBC influences DOC stronger (p < 0.001, ηP = 0.616) than the width (p < 0.001, ηP = 0.398). Significant lower DOC (t test) was measured peripheral compared to center in all materials. Y was more sensitive to the varied parameters as HV. DOC varied among 2.4 mm (SF2, 3-mm offset, exposure distance 7 mm) and 3.9 mm (FO, center, 0 mm).
Whether opacity competes with DOC is material dependent. BF-RBCs tolerate small variations in LCU's centricity better than variations in exposure distance.
The upper incremental thickness threshold of 4 or 5 mm was not reached in all BF-RBCs under simulated clinically relevant curing conditions.
本研究旨在分析现代高粘度大体积充填树脂复合材料(BF-RBC)的不透明度提高是否与固化充分性相矛盾,并评估材料对不太理想固化条件的耐受性。
在一个大腔(10×6)mm 中,用三种 BF-RBC(Filtek One,FO;Tetric Evo Ceram Bulk Fill,TEC-BF; SonicFill2,SF2)一次性充填。在聚合后 24 小时(n=6),以 0.2mm 的步长在 24 小时后在两个中央和两个外围(距中心 4mm)的微机械性能线轮廓(HV,维氏硬度;Y,压痕模量)进行测量。从 HV 深度变化计算出固化深度(DOC)。划痕试验(DOC)模拟临床相关固化条件(曝光距离高达 7mm;中央放置且 LCU 偏移 3mm)时,估计聚合的耐受性。评估了在各种固化条件下使用的光固化器(LCU)的辐照度和光谱分布。
DOC 在 3.6mm(SF2,外围)和 5.7mm(FO,中央)之间变化。BF-RBC 对 DOC 的影响比宽度更强(p<0.001,ηP=0.616)(p<0.001,ηP=0.398)。在所有材料中,与中心相比,外围处的 DOC 显著更低(t 检验)。与 HV 相比,Y 对变化参数更敏感。DOC 在 2.4mm(SF2,3mm 偏移,曝光距离 7mm)和 3.9mm(FO,中心,0mm)之间变化。
不透明度与 DOC 是否竞争取决于材料。BF-RBC 对 LCU 中心性的微小变化比曝光距离的变化更能耐受。
在模拟临床相关固化条件下,所有 BF-RBC 均未达到 4 或 5mm 的上增量厚度阈值。