Baudin Mathieu, Vuichoud Basile, Bornet Aurélien, Bodenhausen Geoffrey, Jannin Sami
Laboratoire des biomolécules, LBM, Département de chimie, École normale supérieure, PSL University, Sorbonne Université, CNRS, 75005 Paris, France.
Université de Lyon, CNRS, Université Claude Bernard Lyon 1, ENS de Lyon, Institut des Sciences Analytiques, UMR 5280, 69100 Villeurbanne, France.
J Magn Reson. 2018 Sep;294:115-121. doi: 10.1016/j.jmr.2018.07.001. Epub 2018 Jul 2.
A novel system for dissolution dynamic nuclear polarization based on a cost-effective "cryogen-free" magnet that can generate fields up to 9.4 T with a sample space that can reach temperatures below 1.4 K in a continuous and stable manner. Polarization levels up to P(H) = 60 ± 5% can be reached with TEMPOL in about 20 min, and P(C) = 50 ± 5% can be achieved using adiabatic cross polarization.
一种基于具有成本效益的“无低温制冷剂”磁体的新型溶解动态核极化系统，该磁体能够产生高达9.4 T的磁场，其样品空间能够以连续且稳定的方式达到低于1.4 K的温度。使用TEMPOL在约20分钟内可达到高达P(H)=60±5%的极化水平，采用绝热交叉极化可实现P(C)=50±5%。
