Department of Biomateirals & Biomimetics, New York University College of Dentistry, New York, NY 10010, United States.
Department of Biomateirals & Biomimetics, New York University College of Dentistry, New York, NY 10010, United States.
J Mech Behav Biomed Mater. 2018 Dec;88:170-175. doi: 10.1016/j.jmbbm.2018.08.023. Epub 2018 Aug 21.
The aim of this study was to evaluate the load-bearing capacity of monolithic lithium disilicate (LiDi - IPS e.max CAD) and novel ultra-translucent zirconia restorative systems of various compositions: 5Y-PSZ (5 mol% yttria-partially-stabilized zirconia) and 4Y-PSZ (4 mol% yttria-partially-stabilized zirconia); relative to a 3Y-TZP (3 mol% yttria-stabilized zirconia) control.
Experiments were carried out with 10 disc specimens (Ø12 ×1 mm) per ceramic material. The zirconia intaglio surface (as machined) was sandblasted (50 µm AlO at 2 bar), while LiDi was etched with 5% HF for 20 s. The ceramic discs were then adhesively bonded onto a dentin-like substrate (G10, a high-pressure fiberglass material) using Multilink Automix cement and Monobond Plus primer, producing a ceramic/cement/dentin-like substrate trilayer structure. The bonded specimens were stored in water for 3 days at 37 °C prior to a Hertzian indentation flexural radial fracture test. The plate-on-foundation theory was used to validate the load-bearing capacity of the trilayer systems based on the flexural tensile stress at the ceramic intaglio (cementation) surface-a cause for bulk fracture of ceramic onlays.
The experiment data showed that, when bonded to and supported by a dentin-like substrate, the load-bearing capacity of LiDi (872 N) is superior to the 5Y-PSZ (715 N) and can even reach that of 4Y-PSZ (864 N), while 3Y-TZP still holds the highest load-bearing capacity (1195 N). Theoretical analyses agree with experimental observations. The translucency of 5Y-PSZ approaches that of LiDi, which are superior to both 4Y-PSZ and 3Y-TZP.
When adhesively bonded to and supported by dentin, lithium disilicate exhibits similar load-bearing properties to 4Y-PSZ but much better than 5Y-PSZ.
本研究旨在评估整体式硅酸锂(LiDi - IPS e.max CAD)和新型超高透光性氧化锆修复体系统的承载能力,这些系统具有不同的组成成分:5Y-PSZ(5 mol%氧化钇部分稳定氧化锆)和 4Y-PSZ(4 mol%氧化钇部分稳定氧化锆);与 3Y-TZP(3 mol%氧化钇稳定氧化锆)对照。
每个陶瓷材料进行 10 个圆盘试件(Ø12×1mm)的实验。氧化锆凹面(机加工)用 50 µm AlO 喷砂处理(2 巴),而 LiDi 则用 5% HF 蚀刻 20 秒。然后,将陶瓷圆盘用 Multilink Automix 水泥和 Monobond Plus 底漆粘合到类似牙本质的基底(G10,一种高压玻璃纤维材料)上,形成陶瓷/水泥/类似牙本质基底三层结构。在 37°C 的水中储存 3 天后,对粘合的试件进行 Hertzian 压痕弯曲径向断裂试验。板基理论用于根据陶瓷凹面(粘结)表面的弯曲拉伸应力来验证三层系统的承载能力-这是陶瓷嵌体整体断裂的原因。
实验数据表明,当粘合并支撑在类似牙本质的基底上时,LiDi(872 N)的承载能力优于 5Y-PSZ(715 N),甚至可以达到 4Y-PSZ(864 N)的水平,而 3Y-TZP 仍然具有最高的承载能力(1195 N)。理论分析与实验观察一致。5Y-PSZ 的透光率接近 LiDi,优于 4Y-PSZ 和 3Y-TZP。
当粘合并支撑在牙本质上时,硅酸锂表现出与 4Y-PSZ 相似的承载性能,但优于 5Y-PSZ。