Tao Jin, Zhang Qiankun, Xiao Yunfeng, Li Xiaoying, Yao Pei, Pang Wei, Zhang Hao, Duan Xuexin, Zhang Daihua, Liu Jing
State Key Laboratory of Precision Measurement Technology and Instruments, School of Precision Instruments and Opto-Electronics Engineering, Tianjin University, Tianjin 300072, China.
State Key Laboratory for Mesoscopic Physics, School of Physics, Peking University, Beijing 100044, China.
Micromachines (Basel). 2016 Feb 25;7(3):36. doi: 10.3390/mi7030036.
We developed a micro-gas detector based on a Fabry-Pérot (FP) cavity embedded in a microfluidic channel. The detector was fabricated in two steps: a silicon substrate was bonded to a glass slide curved with a micro-groove, forming a microfluidic FP cavity; then an optical fiber was inserted through a hole drilled at the center of the groove into the microfluidic FP cavity, forming an FP cavity. The light is partially reflected at the optical fiber endface and the silicon surface, respectively, generating an interference spectrum. The detection is implemented by monitoring the interference spectrum shift caused by the refractive index change of the FP cavity when a gas analyte passes through. This detection mechanism (1) enables detecting a wide range of analytes, including both organic and inorganic (inertia) gases, significantly enhancing its versatility; (2) does not disturb any gas flow so that it can collaborate with other detectors to improve sensing performances; and (3) ensures a fast sensing response for potential applications in gas chromatography systems. In the experiments, we used various gases to demonstrate the sensing capability of the detector and observed drastically different sensor responses. The estimated sensitivity of the detector is 812.5 nm/refractive index unit (RIU) with a detection limit of 1.2 × 10 RIU assuming a 1 pm minimum resolvable wavelength shift.
我们基于嵌入微流控通道的法布里-珀罗(FP)腔开发了一种微型气体探测器。该探测器分两步制造:将硅基片与刻有微槽的弯曲载玻片键合,形成微流控FP腔;然后将一根光纤通过在微槽中心钻出的孔插入微流控FP腔,形成一个FP腔。光分别在光纤端面和硅表面发生部分反射,产生干涉光谱。当气体分析物通过时,通过监测由FP腔折射率变化引起的干涉光谱偏移来实现检测。这种检测机制(1)能够检测多种分析物,包括有机和无机(惰性)气体,显著提高了其通用性;(2)不会干扰任何气流,因此它可以与其他探测器协作以提高传感性能;(3)确保了快速的传感响应,适用于气相色谱系统中的潜在应用。在实验中,我们使用了各种气体来展示探测器的传感能力,并观察到截然不同的传感器响应。假设最小可分辨波长偏移为1 pm,探测器的估计灵敏度为812.5 nm/折射率单位(RIU),检测限为1.2×10 RIU。