Ablett J M, Prieur D, Céolin D, Lassalle-Kaiser B, Lebert B, Sauvage M, Moreno Th, Bac S, Balédent V, Ovono A, Morand M, Gélebart F, Shukla A, Rueff J P
Synchrotron SOLEIL, L'Orme des Merisiers, BP 48, Saint Aubin, 91192 Gif-sur-Yvette, France.
Laboratoire de Physique des Solides, 91400 Orsay, France.
J Synchrotron Radiat. 2019 Jan 1;26(Pt 1):263-271. doi: 10.1107/S160057751801559X.
GALAXIES is an in-vacuum undulator hard X-ray micro-focused beamline dedicated to the study of the electronic structure of materials with high energy resolution using both photoelectron spectroscopy and inelastic X-ray scattering and under both non-resonant (NR-IXS) and resonant (RIXS) conditions. Due to the penetrating power of hard X-rays and the photon-in/photon-out' technique, the sample environment is not a limitation. Materials under extreme conditions, for example in diamond anvil cells or catalysis chambers, thus constitute a major research direction. Here, the design and performance of the inelastic X-ray scattering end-station that operates in the energy range from ∼4 keV up to 12 keV is reported, and its capabilities are highlighted using a selection of data taken from recently performed experiments. The ability to scan on the fly' the incident and scattered/emitted X-ray energies, and the sample position enables fast data collection and high experimental throughput. A diamond X-ray transmission phase retarder, which can be used to generate circularly polarized light, will also be discussed in the light of the recent RIXS-MCD approach.
GALAXIES是一条真空型波荡器硬X射线微聚焦光束线,致力于在非共振(NR-IXS)和共振(RIXS)条件下,利用光电子能谱和非弹性X射线散射,以高能量分辨率研究材料的电子结构。由于硬X射线的穿透能力和“光子入/光子出”技术,样品环境不是一个限制因素。因此,极端条件下的材料,例如金刚石对顶砧或催化室中的材料,构成了一个主要的研究方向。本文报道了在约4 keV至12 keV能量范围内运行的非弹性X射线散射终端站的设计和性能,并通过从最近进行的实验中选取的一些数据突出了其功能。能够“实时”扫描入射和散射/发射的X射线能量以及样品位置,实现了快速数据采集和高实验通量。还将根据最近的RIXS-MCD方法讨论一种可用于产生圆偏振光的金刚石X射线透射相位延迟器。