Kim Jung-Hwan, Moon Seunghyun, Kim Ji-Woong, Lee Donggun, Park Byong Chon, Kim Dal-Hyun, Jeong Yoojin, Hand Sean, Osborne Jason, De Wolf Peter, Kim Youn Sang, Shin ChaeHo
Scientific Instruments Reliability Assessment Center/Smart Open Lab., Korea Basic Science Institute, Daejeon, 34113, Republic of Korea.
Division of Industrial Metrology, Korea Research Institute of Standards and Science, Daejeon, 34113, Republic of Korea.
Sci Rep. 2019 Jan 31;9(1):1018. doi: 10.1038/s41598-018-36991-z.
In current nanoscale semiconductor fabrications, high dielectric materials and ultrathin multilayers have been selected to improve the performance of the devices. Thus, interface effects between films and the quantification of surface information are becoming key issues for determining the performance of the semiconductor devices. In this paper, we developed an easy, accurate, and nondestructive diagnosis to investigate the interface effect of hafnium oxide ultrathin films. A roughness scaling method that artificially modified silicon surfaces with a maximum peak-to-valley roughness range of a few nanometers was introduced to examine the effect on the underlayer roughness. The critical overlayer roughness was be defined by the transition of RMS roughness which was 0.18 nm for the 3 nm thick hafnium oxide film. Subsequently, for the inline diagnostic application of semiconductor fabrication, the roughness of a mass produced hafnium film was investigated. Finally, we confirmed that the result was below the threshold set by our critical roughness. The RMS roughness of the mass produced hafnium oxide film was 0.11 nm at a 500 nm field of view. Therefore, we expect that the quantified and standardized critical roughness managements will contribute to improvement of the production yield.
在当前的纳米级半导体制造中,已选用高介电材料和超薄多层膜来提高器件性能。因此,薄膜之间的界面效应以及表面信息的量化正成为决定半导体器件性能的关键问题。在本文中,我们开发了一种简便、准确且无损的诊断方法来研究氧化铪超薄膜的界面效应。引入了一种粗糙度缩放方法,通过人为地对硅表面进行改性,使其最大峰谷粗糙度范围在几纳米以内,以研究其对下层粗糙度的影响。临界覆盖层粗糙度由均方根粗糙度的转变来定义,对于3纳米厚的氧化铪薄膜,该值为0.18纳米。随后,针对半导体制造的在线诊断应用,对量产铪膜的粗糙度进行了研究。最后,我们确认结果低于我们设定的临界粗糙度阈值。在500纳米视场下,量产氧化铪薄膜的均方根粗糙度为0.11纳米。因此,我们期望量化和标准化的临界粗糙度管理将有助于提高产量。