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掺入5%重量的二氧化钛纳米颗粒对牙科自凝丙烯酸树脂弯曲强度、显微硬度、表面粗糙度和吸水性的影响

Influence of Incorporating 5% Weight Titanium Oxide Nanoparticles on Flexural Strength, Micro-Hardness, Surface Roughness and Water Sorption of Dental Self-Cured Acrylic Resin.

作者信息

Abdelraouf Rasha M, Bayoumi Rania E, Hamdy Tamer M

机构信息

Biomaterials Department, Faculty of Dentistry, Cairo University, Cairo 11553, Egypt.

Biomaterials Department, Faculty of Dentistry (Girls), Azhar University, Cairo 11754, Egypt.

出版信息

Polymers (Basel). 2022 Sep 8;14(18):3767. doi: 10.3390/polym14183767.

Abstract

BACKGROUND

Polymethyl methacrylate (PMMA) is used in fabricating acrylic denture bases. Repairing a fractured acrylic denture base can be done by self-cured PMMA, yet this is still a weak point after repair. The aim of this study was to evaluate the effect of incorporating 5% weight titanium oxide nanoparticles (TiO) to self-cured PMMA on flexural strength, surface micro-hardness, roughness, and water sorption.

METHODS

A total of 160 acrylic-resin specimens were used in this study. They were divided in two main groups; (a) control group, prepared by mixing self-cured PMMA powder to its liquid monomer, (b) treated group, prepared by blending 5% weight TiO nanoparticles to self-cured PMMA powder then this blend was mixed with the liquid monomer. Flexure strength, surface micro-hardness, roughness, and water sorption were evaluated. Data were analyzed using independent sample -tests ( ≤ 0.05).

RESULTS

There was a significant increase in the flexural strength of PMMA of the treated group after the addition of TiO (137.6 MPa) compared with the control (75.4 MPa) ( ≤ 0.001). No significant difference between the two groups in terms of micro-hardness ( = 0.385) and surface roughness ( = 0.269). Water sorption showed a significant reduction in the treated group ( ≤ 0.001).

CONCLUSIONS

Addition of 5% weight TiO nanoparticles to the self-cured acrylic resin improved its flexural strength and reduced its water-sorption without impairing the surface micro-hardness and roughness.

摘要

背景

聚甲基丙烯酸甲酯(PMMA)用于制作丙烯酸义齿基托。用自凝PMMA修复断裂的丙烯酸义齿基托是可行的,但修复后仍是一个薄弱环节。本研究的目的是评估在自凝PMMA中加入5%重量的二氧化钛纳米颗粒(TiO)对弯曲强度、表面显微硬度、粗糙度和吸水性的影响。

方法

本研究共使用了160个丙烯酸树脂标本。它们被分为两个主要组;(a)对照组,通过将自凝PMMA粉末与液态单体混合制备;(b)处理组,通过将5%重量的TiO纳米颗粒与自凝PMMA粉末混合,然后将该混合物与液态单体混合制备。评估弯曲强度、表面显微硬度、粗糙度和吸水性。使用独立样本检验(≤0.05)分析数据。

结果

与对照组(75.4MPa)相比,添加TiO后处理组PMMA的弯曲强度显著增加(137.6MPa)(≤0.001)。两组在显微硬度(=0.385)和表面粗糙度(=0.269)方面无显著差异。处理组的吸水性显著降低(≤0.001)。

结论

在自凝丙烯酸树脂中添加5%重量的TiO纳米颗粒可提高其弯曲强度并降低其吸水性,而不会损害表面显微硬度和粗糙度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/173d/9502913/706b586da0e0/polymers-14-03767-g001.jpg

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