Peterson Jana, Rizk Marta, Hoch Monika, Wiegand Annette
Department of Preventive Dentistry, Periodontology and Cariology, University of Goettingen, Robert-Koch-Str. 40, 37075, Göttingen, Germany.
Odontology. 2018 Apr;106(2):171-180. doi: 10.1007/s10266-017-0324-3. Epub 2017 Dec 14.
This study aimed to analyze bond strengths of self-adhesive flowable composites on enamel, dentin and nano-hybrid composite. Enamel, dentin and nano-hybrid composite (Venus Diamond, Heraeus Kulzer, Germany) specimens were prepared. Three self-adhesive composites (Constic, DMG, Germany; Fusio Liquid Dentin, Pentron Clinical, USA; Vertise Flow, Kerr Dental, Italy) or a conventional flowable composite (Venus Diamond Flow, Heraeus Kulzer, Germany, etch&rinse technique) were applied to enamel and dentin. Nano-hybrid composite specimens were initially aged by thermal cycling (5000 cycles, 5-55 °C). Surfaces were left untreated or pretreated by mechanical roughening, AlO air abrasion or silica coating/silanization. In half of the composite specimens, an adhesive (Optibond FL, Kerr Dental, Italy) was used prior to the application of the flowable composites. Following thermal cycling (5000 cycles, 5-55 °C) of all specimens, shear bond strengths (SBS) and failure modes were analyzed (each subgroup n = 16). Statistical analysis was performed by ANOVAs/Bonferroni post hoc tests, Weibull statistics and χ -tests (p < 0.05). SBS (MPa) of the self-adhesive composites on enamel and dentin were significantly lower (enamel: < 5, dentin: < 3) than those of the conventional flowable composite (enamel: 13.0 ± 5.1, dentin: 11.2 ± 6.3), and merely adhesive failures could be observed. On the nano-hybrid composite, SBS were significantly related to the pretreatment. Adhesive application improved SBS of the conventional, but not of the self-adhesive composites. The self-adhesive composite groups showed less cohesive failures than the reference group; the occurence of cohesive failures increased after surface pretreatment. Bonding of self-adhesive flowable composites to enamel and dentin is lower than bonding to a nano-hybrid composite.
本研究旨在分析自粘性可流动复合树脂与牙釉质、牙本质及纳米混合复合树脂之间的粘结强度。制备了牙釉质、牙本质及纳米混合复合树脂(德国贺利氏古莎公司的Venus Diamond)样本。将三种自粘性复合树脂(德国DMG公司的Constic、美国Pentron Clinical公司的Fusio Liquid Dentin、意大利登士柏公司的Vertise Flow)或一种传统可流动复合树脂(德国贺利氏古莎公司的Venus Diamond Flow,酸蚀冲洗技术)应用于牙釉质和牙本质。纳米混合复合树脂样本首先进行热循环老化(5000次循环,5 - 55°C)。表面不做处理或通过机械粗化、AlO空气喷砂或二氧化硅涂层/硅烷化进行预处理。在一半的复合树脂样本中,在应用可流动复合树脂之前使用了一种粘结剂(意大利登士柏公司的Optibond FL)。对所有样本进行热循环(5000次循环,5 - 55°C)后,分析剪切粘结强度(SBS)和失效模式(每个亚组n = 16)。通过方差分析/邦费罗尼事后检验、威布尔统计和χ检验进行统计分析(p < 0.05)。自粘性复合树脂在牙釉质和牙本质上的SBS(MPa)显著低于传统可流动复合树脂(牙釉质:< 5,牙本质:< 3)(牙釉质:13.0 ± 5.1,牙本质:11.2 ± 6.3),且仅观察到粘结性失效。在纳米混合复合树脂上,SBS与预处理显著相关。使用粘结剂提高了传统复合树脂的SBS,但未提高自粘性复合树脂的SBS。自粘性复合树脂组的内聚性失效比对照组少;表面预处理后内聚性失效的发生率增加。自粘性可流动复合树脂与牙釉质和牙本质的粘结低于与纳米混合复合树脂的粘结。