Satzinger G, Herrmann W, Zimmermann F
Arzneimittelforschung. 1975;25(12):1849-53.
Physico-chemical, spectroscopic (UV, IR, NMR, mass), chromatographic (GLC, TLC) properties and synthesis of 1,3-bis(2-ethylhexyl)-5-amino-5-methyl-hexahydropyrimidine (hexetidine) are reported and discussed. Moreover, the difference between commercial and purified hexetidine is demonstrated.
报道并讨论了1,3-双(2-乙基己基)-5-氨基-5-甲基六氢嘧啶(己脒定)的物理化学、光谱(紫外、红外、核磁共振、质谱)、色谱(气相色谱、薄层色谱)性质及合成方法。此外,还展示了市售己脒定与纯化己脒定之间的差异。