Suppr超能文献

阿拉伯树胶包覆的铜纳米粒子:合成、表征及应用。

Gum arabic capped copper nanoparticles: Synthesis, characterization, and applications.

机构信息

Shoolini University, Solan, Himachal Pradesh, India.

Amity University, Jaipur, Rajasthan, India.

出版信息

Int J Biol Macromol. 2020 Mar 1;146:232-242. doi: 10.1016/j.ijbiomac.2019.12.260. Epub 2020 Jan 2.

Abstract

In present work, we synthesized copper nanoparticles using l-ascorbic acid as a reducing agent and capped them with gum arabic. Based upon spectrometric analysis and particle size distribution (19.60-35.06 nm) by intensity, a 1% concentration of gum arabic was selected as the suitable capping agent for copper nanoparticles. Gum arabic capped copper nanoparticles revealed significantly (p < 0.05) higher zeta potential value than that of unmodified copper nanoparticles. Energy-dispersive X-ray spectroscopy revealed the purity of the copper nanoparticles, whereas scanning electron microscopy confirmed the polygonal prismatic shape of the gum arabic capped copper nanoparticles. As well, TEM analysis confirmed the monodispersed nature of the gum arabic capped copper nanoparticles. Gum arabic capped copper nanoparticles showed significantly (p < 0.05) higher zone of inhibition for Salmonella typhimurium (27 mm) than that of other bacterial strains. Approximately 95% photocatalytic degradation of methylene blue and crystal violet was observed within 40 and 20 min. As well, both unmodified and gum arabic capped copper nanoparticles were found to be non-toxic to Caco-2 cells during cell viability assay.

摘要

在本工作中,我们使用抗坏血酸作为还原剂合成了铜纳米粒子,并以阿拉伯胶作为稳定剂。根据光谱分析和基于强度的粒径分布(19.60-35.06nm),选择 1%浓度的阿拉伯胶作为铜纳米粒子的合适稳定剂。与未修饰的铜纳米粒子相比,阿拉伯胶稳定的铜纳米粒子具有显著更高的(p<0.05)zeta 电位值。能谱分析揭示了铜纳米粒子的纯度,而扫描电子显微镜则证实了阿拉伯胶稳定的铜纳米粒子具有多面棱柱形的形状。此外,TEM 分析证实了阿拉伯胶稳定的铜纳米粒子具有单分散性。阿拉伯胶稳定的铜纳米粒子对鼠伤寒沙门氏菌(27mm)的抑菌圈明显(p<0.05)高于其他菌株。在 40 和 20 分钟内,观察到亚甲基蓝和结晶紫的光催化降解率分别约为 95%。此外,在细胞活力测定中,未修饰和阿拉伯胶稳定的铜纳米粒子均被发现对 Caco-2 细胞无毒。

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验