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义齿基托复合材料:表面改性纳米和微米颗粒对聚甲基丙烯酸甲酯力学性能的影响

Denture Base Composites: Effect of Surface Modified Nano- and Micro-Particulates on Mechanical Properties of Polymethyl Methacrylate.

作者信息

Nejatian Touraj, Nathwani Neil, Taylor Louise, Sefat Farshid

机构信息

Eastman Dental Institute, University College London, London WC1X 8WD, UK.

Department of Biomedical and Electronics Engineering, School of Engineering, University of Bradford, Bradford BD7 1DP, UK.

出版信息

Materials (Basel). 2020 Jan 9;13(2):307. doi: 10.3390/ma13020307.

Abstract

The most commonly used denture base material, polymethyl methacrylate, lacks ideal mechanical properties, which are reflected in its relatively high failure rate. Several methods have been explored to reinforce the material and reduce the cost of denture repair and replacement. In this study, various surface modified filler particles at different concentrations were dispersed in conventional and high-impact denture base materials and tested for their improvement in mechanical properties. Inorganic filler particles were coated with different silane coupling agents using an ultrasonic device. The particulates were dispersed in the resin and the composites polymerised through an innovative dual-cure technique. Charpy impact test, single-edge notch three-point bend fracture toughness test and Biaxial Flexural Strength (BFS) were performed on the specimens. The results showed that mechanical properties of the denture base resin can be improved by incorporating filler particles; however, the surface characteristics, quantity and level of dispersion of the particles play critical role in the mechanical behaviour of the composites. The results of this study are a promising step towards developing more fracture-resistant denture base materials.

摘要

最常用的义齿基托材料聚甲基丙烯酸甲酯缺乏理想的机械性能,这体现在其相对较高的失败率上。人们已经探索了几种方法来增强这种材料,并降低义齿修复和更换的成本。在本研究中,将不同浓度的各种表面改性填料颗粒分散在传统和高抗冲义齿基托材料中,并测试它们在机械性能方面的改善情况。使用超声设备用不同的硅烷偶联剂对无机填料颗粒进行包覆。将颗粒分散在树脂中,并通过创新的双重固化技术使复合材料聚合。对试样进行夏比冲击试验、单边切口三点弯曲断裂韧性试验和双轴弯曲强度(BFS)测试。结果表明,通过加入填料颗粒可以改善义齿基托树脂的机械性能;然而,颗粒的表面特性、数量和分散程度在复合材料的力学行为中起着关键作用。本研究结果是朝着开发更抗断裂的义齿基托材料迈出的有希望的一步。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/02d6/7013693/2fb53154b6b5/materials-13-00307-g001.jpg

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