Sharayei Parvin, Azarpazhooh Elham, Ramaswamy Hosahalli S
Agricultural Engineering Research Department, Khorasan Razavi Agricultural and Natural Resources Research and Education Center, AREEO, PO Box 488, Mashhad, Iran.
2Department of Food Science and Agricultural Chemistry, Macdonald Campus of McGill University, 21111 Lakeshore Road, Ste. Anne de Bellevue, QC H9X 3V9 Canada.
J Food Sci Technol. 2020 Feb;57(2):723-733. doi: 10.1007/s13197-019-04105-w. Epub 2019 Sep 16.
The aqueous extract of pomegranate ( L.) peel compounds was freeze-dried (FDPOPx) and encapsulated using two wall forming components at two concentrations (maltodextrin: MDX and β-cyclodextrin: βCDX; 5 and 10%) with a mass ratio of 1:5 (extract/wall material). Different properties of the encapsulated powders (bioactive components, physicochemical and morphological properties) and storage stability of prepared microcapsules were evaluated during 42 days of storage at a different relative humidity (52 and 75%) and temperatures (4 and 25 °C). Encapsulated powder with βCDX-10% had the highest total phenolic compounds (TPC: 58.78 mg GA/g) and antioxidant capacity [FRAP: 1414.76 μmol Fe/g and DPPH assay (RSA): 77.83%] among other wall materials. The amounts of TPC and their antioxidant capacity decreased during the 42 days of storage. However, the highest TPC was observed in the freeze-dried MDX-10% % encapsulated powder at 4 °C storage temperature and 52% relative humidity with a half-life (t) of 81 days, the reaction rate constant (k) of 0.85 × 10 min and the glass transition temperature of 69.73 °C. In addition, the polyphenolic extracts (both free and encapsulated) were able to control the growth of yeasts and molds, and maintaining the sensory properties of cupcakes as the model food system. The lowest growth after 9 days of storage of cupcake was observed in samples prepared with 1.5% of microencapsulated powder (MDX-10%) which was equivalent to the effect of the chemical preservative potassium sorbate.
石榴(L.)果皮化合物的水提取物经冷冻干燥(FDPOPx),并使用两种壁材成分在两种浓度(麦芽糊精:MDX和β-环糊精:βCDX;5%和10%)下以质量比1:5(提取物/壁材)进行包封。在不同相对湿度(52%和75%)和温度(4℃和25℃)下储存42天期间,评估了包封粉末的不同性质(生物活性成分、物理化学和形态学性质)以及制备的微胶囊的储存稳定性。在其他壁材中,含10%βCDX的包封粉末具有最高的总酚化合物含量(TPC:58.78毫克没食子酸/克)和抗氧化能力[铁还原抗氧化能力测定法(FRAP):1414.76微摩尔铁/克,二苯基苦味酰基自由基测定法(RSA):77.83%]。在储存的42天期间,TPC的含量及其抗氧化能力有所下降。然而,在4℃储存温度和52%相对湿度下,含10%MDX的冷冻干燥包封粉末中观察到最高的TPC,其半衰期(t)为81天,反应速率常数(k)为0.85×10⁻²分钟⁻¹,玻璃化转变温度为69.73℃。此外,多酚提取物(游离和包封的)能够控制酵母和霉菌的生长,并保持作为模型食品体系的纸杯蛋糕的感官特性。在用1.5%微胶囊粉末(MDX - 10%)制备的样品中,观察到纸杯蛋糕储存9天后的生长最低,这与化学防腐剂山梨酸钾的效果相当。