Singh Sunpreet, Prakash Chander, Pramanik Alokesh, Basak Animesh, Shabadi Rajasekhara, Królczyk Grzegorz, Bogdan-Chudy Marta, Babbar Atul
Department of Mechanical Engineering, National University of Singapore, Singapore 119077, Singapore.
School of Mechanical Engineering, Lovely Professional University, Phagwara, Punjab 144411, India.
Materials (Basel). 2020 Nov 16;13(22):5156. doi: 10.3390/ma13225156.
The present work explores the potential of magneto-rheological fluid assisted abrasive finishing (MRF-AF) for obtaining precise surface topography of an in-house developed β-phase Ti-Nb-Ta-Zr (TNTZ) alloy for orthopedic applications. Investigations have been made to study the influence of the concentration of carbonyl iron particles (CIP), rotational speed (Nt), and working gap (Gp) in response to material removal (MR) and surface roughness (Ra) of the finished sample using a design of experimental technique. Further, the corrosion performance of the finished samples has also been analyzed through simulated body fluid (SBF) testing. It has been found that the selected input process parameters significantly influenced the observed MR and Ra values at 95% confidence level. Apart from this, it has been found that Gp and Nt exhibited the maximum contribution in the optimized values of the MR and Ra, respectively. Further, the corrosion analysis of the finished samples specified that the resistance against corrosion is a direct function of the surface finish. The morphological analysis of the corroded morphologies indicated that the rough sites of the implant surface have provided the nuclei for corrosion mechanics that ultimately resulted in the shredding of the appetite layer. Overall results highlighted that the MRF-AF is a potential technique for obtaining nano-scale finishing of the high-strength β-phase Ti-Nb-Ta-Zr alloy.
本研究探讨了磁流变液辅助研磨加工(MRF-AF)在获得用于骨科应用的自行研发的β相Ti-Nb-Ta-Zr(TNTZ)合金精确表面形貌方面的潜力。采用实验设计技术,研究了羰基铁颗粒(CIP)浓度、转速(Nt)和工作间隙(Gp)对加工后样品的材料去除率(MR)和表面粗糙度(Ra)的影响。此外,还通过模拟体液(SBF)测试分析了加工后样品的耐腐蚀性能。结果发现,所选的输入工艺参数在95%置信水平下对观察到的MR和Ra值有显著影响。除此之外,还发现Gp和Nt分别在MR和Ra的优化值中贡献最大。进一步的加工后样品腐蚀分析表明,耐腐蚀性能是表面光洁度的直接函数。腐蚀形貌的形态分析表明,植入物表面的粗糙部位为腐蚀机制提供了核心,最终导致了表层的剥落。总体结果表明,MRF-AF是一种获得高强度β相Ti-Nb-Ta-Zr合金纳米级加工的潜在技术。