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用于常规、减法和加法制造咬合设备的聚合物在硬度和弯曲性能上有所不同,但在耐磨性方面没有区别。

Polymers for conventional, subtractive, and additive manufacturing of occlusal devices differ in hardness and flexural properties but not in wear resistance.

机构信息

Medical Center - University of Freiburg, Center for Dental Medicine, Department of Prosthetic Dentistry, Faculty of Medicine, University of Freiburg, Hugstetter Str. 55, 79106 Freiburg, Germany; Department of Prosthodontics, Geriatric Dentistry and Craniomandibular Disorders, Charité - Universitätsmedizin Berlin, Corporate Member of Freie Universität Berlin, Humboldt-Universität zu Berlin and Berlin Institute of Health, Assmanshauser Str. 4-6, 14197 Berlin, Germany.

Medical Center - University of Freiburg, Center for Dental Medicine, Department of Prosthetic Dentistry, Faculty of Medicine, University of Freiburg, Hugstetter Str. 55, 79106 Freiburg, Germany.

出版信息

Dent Mater. 2021 Mar;37(3):432-442. doi: 10.1016/j.dental.2020.11.020. Epub 2020 Dec 4.

Abstract

OBJECTIVES

To investigate the wear resistance of polymers for injection molding, subtractive and additive manufacturing of occlusal devices in comparison with enamel antagonist wear and material properties (i.e., hardness, flexural strength, and flexural modulus).

METHODS

Injection molding was compared with milling and the additive technologies stereolithography, low force stereolithography, and digital light processing. For each material, eight specimens were produced for wear measurements. Extracted human premolars served as indenters. All samples were subjected to two series of a 2-body wear test consisting of 200,000 circular loading cycles with an applied load of 1) 20 N and 2) 50 N in a thermocycling environment (5/55 °C, 30 s, 3860 cycles, HO). Wear resistance was characterized by means of maximum depth and volume of the resulting traces. In addition, enamel wear of the indenters and Vickers hardness, flexural strength, and flexural modulus of the polymers were determined. Wear was statistically analyzed with linear general models for repeated measures and material properties with one-way ANOVA with post-hoc Tukey-HSD tests.

RESULTS

Wear of the antagonists was not influenced by the material (P ≥ 0.343). Likewise, no differences in wear resistance were found between materials after cyclic loading with 20 N or 50 N (P ≥ 0.074). Material properties investigated revealed decreased values for the resins for the additive manufacturing with the exception of flexural strength of one material.

SIGNIFICANCE

Within the limitations of this in-vitro study, arylates for conventional, subtractive, and additive manufacturing of occlusal devices differ in material properties but not in wear resistance and antagonist wear.

摘要

目的

研究注塑、减法和加法制造的用于制作咬合装置的聚合物的耐磨性,与牙釉质对磨耗和材料特性(即硬度、弯曲强度和弯曲模量)进行比较。

方法

注塑与铣削以及立体光固化、低力立体光固化和数字光处理等加法技术进行了比较。对于每种材料,都制作了八个样本进行磨损测量。提取的人前磨牙用作压头。所有样品均进行了两个 2 体磨损测试系列,包括 200000 次循环的圆形加载,施加的负载为 1)20N 和 2)50N,在热循环环境(5/55°C,30s,3860 次循环,HO)中。通过产生痕迹的最大深度和体积来表征耐磨性。此外,还确定了压头的牙釉质磨损和聚合物的维氏硬度、弯曲强度和弯曲模量。使用线性重复测量广义模型对磨损进行统计分析,使用单向方差分析和事后 Tukey-HSD 检验对材料特性进行分析。

结果

材料对拮抗物的磨损没有影响(P≥0.343)。同样,在循环加载 20N 或 50N 后,材料之间的耐磨性也没有差异(P≥0.074)。所研究的材料性能显示,除了一种材料的弯曲强度外,用于加法制造的树脂的数值降低。

意义

在本体外研究的限制范围内,用于常规、减法和加法制造咬合装置的芳基酯在材料性能上存在差异,但在耐磨性和拮抗物磨损方面没有差异。

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