Freitas Filipa, Pinheiro de Melo Teresa, Delgado António Hs, Monteiro Paulo, Rua João, Proença Luís, Caldeira Jorge, Mano Azul Ana, Mendes José João
Clinical Research Unit (CRU), Centro de Investigação Interdisciplinar Egas Moniz (CiiEM), Instituto Universitário Egas Moniz (IUEM), 2829-511 Almada, Portugal.
Department of Biomaterials and Tissue Engineering, Royal Free Hospital, UCL Eastman Dental Institute, London NW3 NPF, UK.
J Funct Biomater. 2020 Dec 22;12(1):1. doi: 10.3390/jfb12010001.
Surface properties of composites such as roughness and color impact periodontal health and aesthetic outcomes. Novel bulk-fill composites with improved functionality are being introduced and, in light of the existing variety of finishing/polishing procedures, research of their surface properties is warranted. Sixty discs were prepared from bulk-fill composites (Filtek™ Bulk Fill Posterior Restorative and Fill-Up™) and incremental-fill Filtek™ Z250. They were further divided according to different polishing procedures ( = 5): three multi-step polishing procedures or finishing with a bur (control). Surface roughness (Ra) was measured using an atomic force microscope (The AFM Workshop TT-AFM). A spectrophotometer (Spectroshade Micro Optic) was used to determine color stability, after exposure to a coffee solution. Data were analyzed using two-way MANOVA (significance level of 5%). Resin composite type, polishing procedure, and their interaction had a statistically significant effect on surface roughness ( < 0.001) and color change ( < 0.001). Fill-Up™ exhibited the highest surface roughness and greatest color change. Differences in color change were statistically significant ( < 0.001). Filtek™ Bulk Fill registered the lowest surface roughness and color change, after the three-step polishing procedure. Both parameters were significantly correlated (ρ = 0.754, < 0.001) and found to be material dependent and polishing-procedure dependent. Higher surface roughness relates to greater color changes.
复合材料的表面特性,如粗糙度和颜色,会影响牙周健康和美学效果。具有改进功能的新型大块充填复合材料不断推出,鉴于现有的各种修整/抛光程序,对其表面特性进行研究是必要的。从大块充填复合材料(Filtek™ Bulk Fill Posterior Restorative和Fill-Up™)以及分层充填的Filtek™ Z250制备了60个圆盘。它们根据不同的抛光程序(每组n = 5)进一步划分:三种多步抛光程序或用车针修整(对照)。使用原子力显微镜(The AFM Workshop TT-AFM)测量表面粗糙度(Ra)。使用分光光度计(Spectroshade Micro Optic)在暴露于咖啡溶液后测定颜色稳定性。使用双向多变量方差分析(显著性水平为5%)分析数据。树脂复合材料类型、抛光程序及其相互作用对表面粗糙度(P < 0.001)和颜色变化(P < 0.001)具有统计学显著影响。Fill-Up™表现出最高的表面粗糙度和最大的颜色变化。颜色变化的差异具有统计学显著性(P < 0.001)。经过三步抛光程序后,Filtek™ Bulk Fill的表面粗糙度和颜色变化最低。这两个参数显著相关(ρ = 0.754,P < 0.001),并且发现它们取决于材料和抛光程序。较高的表面粗糙度与较大的颜色变化相关。