Hoppe Viktoria, Szymczyk-Ziółkowska Patrycja, Rusińska Małgorzata, Dybała Bogdan, Poradowski Dominik, Janeczek Maciej
Centre for Advanced Manufacturing Technologies-Fraunhofer Project Center, Department of Laser Technologies, Automation and Production Management, Faculty of Mechanical Engineering, Wrocław University of Science and Technology, 50-371 Wrocław, Poland.
Department of Animal Physiology and Biostructure, Division of Anatomy, Faculty of Veterinary Medicine, Wrocław University of Environmental and Life Sciences, 50-375 Wrocław, Poland.
Materials (Basel). 2020 Dec 30;14(1):126. doi: 10.3390/ma14010126.
The purpose of this work is to obtain comprehensive reference data of the Ti-13Nb-13Zr alloy base material: its microstructure, mechanical, and physicochemical properties. In order to obtain extensive information on the tested materials, a number of examination methods were used, including SEM, XRD, and XPS to determine the phases occurring in the material, while mechanical properties were verified with static tensile, compression, and bending tests. Moreover, the alloy's corrosion resistance in Ringer's solution and the cytotoxicity were investigated using the MTT test. Studies have shown that this alloy has the structure α', α, and β phases, indicating that parts of the β phase transformed to α', which was confirmed by mechanical properties and the shape of fractures. Due to the good mechanical properties (E = 84.1 GPa), high corrosion resistance, as well as the lack of cytotoxicity on MC3T3 and NHDF cells, this alloy meets the requirements for medical implant materials. Ti-13Nb-13Zr alloy can be successfully used in implants, including bone tissue engineering products and dental applications.
这项工作的目的是获取Ti-13Nb-13Zr合金基材的全面参考数据:其微观结构、力学性能和物理化学性能。为了获得有关测试材料的广泛信息,使用了多种检测方法,包括扫描电子显微镜(SEM)、X射线衍射(XRD)和X射线光电子能谱(XPS)来确定材料中出现的相,同时通过静态拉伸、压缩和弯曲试验验证力学性能。此外,使用MTT试验研究了该合金在林格氏溶液中的耐腐蚀性和细胞毒性。研究表明,该合金具有α'、α和β相结构,表明部分β相转变为α',这通过力学性能和断口形状得到了证实。由于具有良好的力学性能(弹性模量E = 84.1 GPa)、高耐腐蚀性以及对MC3T3和人正常皮肤成纤维细胞(NHDF)无细胞毒性,该合金符合医用植入材料的要求。Ti-13Nb-13Zr合金可成功用于植入物,包括骨组织工程产品和牙科应用。