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采用绿色溶剂的高强度超声辅助从嘉宝果副产物中回收花色苷:超声强度和溶剂组成对酚类化合物提取的影响。

High-intensity ultrasound-assisted recovery of anthocyanins from jabuticaba by-products using green solvents: Effects of ultrasound intensity and solvent composition on the extraction of phenolic compounds.

机构信息

LANUM (Laboratory of Nutrition and Metabolism)/FEA (School of Food Engineering)/UNICAMP (University of Campinas); Rua Monteiro Lobato, 80, Campinas-SP CEP:13083-862, Brazil.

LASEFI/DEA/FEA (School of Food Engineering)/UNICAMP (University of Campinas), Rua Monteiro Lobato, 80, Campinas-SP CEP:13083-862, Brazil.

出版信息

Food Res Int. 2021 Feb;140:110048. doi: 10.1016/j.foodres.2020.110048. Epub 2021 Jan 8.

Abstract

This study proposes an update for the jabuticaba processing chain to obtain valuable coproducts from jabuticaba peels. High-intensity ultrasound (HIUS) technology was evaluated as a more efficient extraction process to obtain two high added-value coproducts: pectin and an anthocyanins-rich extract. The HIUS-assisted extraction of bioactive compounds like anthocyanins from the jabuticaba peels was evaluated. The effects of ultrasound intensity (1.1, 3.7, 7.3, and 13.0 W/cm) and solvent composition concerning water/ethanol ratio (0, 25, 50, 75, and 100 g water/100 g) were examined. One-step HIUS processing promoted the best recovery of bioactive compounds at an ultrasound intensity of 3.7 W/cm and 50 g water/100 g, thus proofing the interaction between ultrasound intensity and the solvent composition has a strong influence on the extraction efficiency of the groups of compounds studied and in the jabuticaba peel antioxidant potential. The confocal laser scanning microscopy confirmed bioactive compounds' exhaustion in the dried jabuticaba peel after the HIUS processing, proving its best recovery. The jabuticaba peel extract exhibited an intense reddish color typical of anthocyanin-rich products at acid pH (4.5). The HIUS technology turned out a promising way to recover these valuable phenolic compounds as a quick, relatively inexpensive, and simple technology that improves the yields and decreases the costs and environmental impacts compared to conventional extraction processes.

摘要

本研究提出了一种更新的 jabuticaba 加工链,以从 jabuticaba 果皮中获得有价值的副产物。高强度超声(HIUS)技术被评估为一种更有效的提取工艺,可获得两种高附加值的副产物:果胶和富含花色苷的提取物。评估了 HIUS 辅助提取 jabuticaba 果皮中生物活性化合物(如花色苷)的效果。考察了超声强度(1.1、3.7、7.3 和 13.0 W/cm)和溶剂组成(水/乙醇比为 0、25、50、75 和 100 g 水/100 g)对花色苷等生物活性化合物提取的影响。一步 HIUS 处理在超声强度为 3.7 W/cm 和 50 g 水/100 g 时促进了生物活性化合物的最佳回收,证明超声强度和溶剂组成之间的相互作用对所研究化合物组和 jabuticaba 果皮抗氧化能力的提取效率有很强的影响。共焦激光扫描显微镜证实 HIUS 处理后干燥的 jabuticaba 果皮中生物活性化合物已耗尽,证明其得到了最佳回收。jabuticaba 果皮提取物在酸性 pH(4.5)下显示出富含花色苷产品的强烈红色调。HIUS 技术是一种很有前途的回收这些有价值的酚类化合物的方法,与传统提取工艺相比,它是一种快速、相对廉价且简单的技术,可以提高产量,降低成本和环境影响。

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