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使用电感耦合等离子体质谱仪(ICP-MS)、气相色谱-串联质谱仪(GC-MS-MS)和直接实时质谱仪(DART-MS)对(Forssk)茎成分进行化学成分鉴定和金属测定

Identification of Chemical Composition and Metal Determination of (Forssk) Stem Constituents Using ICP-MS, GC-MS-MS, and DART-MS.

作者信息

Al-Onazi Wedad, Al-Mohaimeed Amal M, Amina Musarat, El-Tohamy Maha F

机构信息

Department of Chemistry, College of Science, King Saud University, Riyadh 11451, Saudi Arabia.

Department of Pharmacognosy, College of Pharmacy, King Saud University, Riyadh 11451, Saudi Arabia.

出版信息

J Anal Methods Chem. 2021 Feb 24;2021:6667238. doi: 10.1155/2021/6667238. eCollection 2021.

Abstract

This study aims to investigate the chemical constituents of the stem of growing in Saudi Arabia. The organic and inorganic composition of ethanol extract of stem has been explored using direct analysis in real time-mass spectrometry (DART-MS), gas chromatography-mass spectrometry (GC-MS), and inductively coupled plasma-mass spectrometry (ICP-MS). Analysis conducted by DART-MS and GC-MS reveals the presence of several interesting organic constituents identified as 2,4-di-tert-butylphenol, sparteine, benzenepropanoic acid, 3,5-bis(1,1-dimethylethyl)-4-hydroxy-, methyl ester, phthalic acid, 1-octadecanol, squalene, argentamin, 2,4-di-tert-butylphenol, sparteine, benzene propanoic acid, 3,5-bis(1,1-dimethylethyl)-4-hydroxy-, methyl ester, phthalic acid, 1-octadecanol, squalene, argentamin, and hentriacontane in the ethanol extract of the stem. The ICP-MS analysis of stem extract showed the presence of a significant amount of important inorganic elements including aluminum, chlorine, calcium, bromine magnesium, phosphorus, scandium, and chromium. The current study complements other extract investigations carried out in the past and provides the additional data for the future research studies.

摘要

本研究旨在调查生长于沙特阿拉伯的[植物名称]茎的化学成分。已使用实时直接分析质谱法(DART-MS)、气相色谱-质谱联用法(GC-MS)和电感耦合等离子体质谱法(ICP-MS)对[植物名称]茎乙醇提取物的有机和无机成分进行了探究。通过DART-MS和GC-MS进行的分析表明,在[植物名称]茎乙醇提取物中存在几种有趣的有机成分,鉴定为2,4-二叔丁基苯酚、鹰爪豆碱、苯丙酸、3,5-双(1,1-二甲基乙基)-4-羟基-甲酯、邻苯二甲酸、1-十八烷醇、角鲨烯、银胺、2,4-二叔丁基苯酚、鹰爪豆碱、苯丙酸、3,5-双(1,1-二甲基乙基)-4-羟基-甲酯、邻苯二甲酸、1-十八烷醇、角鲨烯、银胺和三十一烷。对[植物名称]茎提取物的ICP-MS分析表明,存在大量重要的无机元素,包括铝、氯、钙、溴、镁、磷、钪和铬。本研究补充了过去进行的其他[植物名称]提取物研究,并为未来的研究提供了更多数据。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6ae5/7929692/123faf62e067/JAMC2021-6667238.001.jpg

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