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基于离子迁移谱的实时气体监测系统,用于工作场所环境测量。

A real-time gas monitoring system based on ion mobility spectrometry for workplace environmental measurements.

机构信息

National Institute of Occupational Safety and Health, Japan.

High Energy Accelerator Research Organization, KEK, Japan.

出版信息

Ind Health. 2022 Feb 8;60(1):40-46. doi: 10.2486/indhealth.2021-0037. Epub 2021 Nov 8.

Abstract

A volatile organic compounds (VOC) gas monitor was developed using an ion mobility spectrometer (IMS). It was designed for real-time monitoring in work environments, where gas chromatography/mass spectrometry (GC/MS) does not perform well. To evaluate the identification capability, response time, and quantitative accuracy of this device, experiments were conducted using methyl ethyl ketone. This is widely used in many factories, and its short-term exposure limit (STEL) has been set by the American Conference of Governmental Industrial Hygienists. Because the ionizable amount of methyl ethyl ketone has already been exceeded in STEL value of 300 ppm which belongs to the measurement range of interest in this study, this study estimated the peak shift amount rather than the peak intensity. Calibration curves with high accuracy were obtained in a range including 300 ppm which is the STEL of methyl ethyl ketone. The results of the experiment suggest that the device can be used for monitoring chemical substances in a work environment.

摘要

研制了一种使用离子迁移谱仪(IMS)的挥发性有机化合物(VOC)气体监测器。它专为工作环境中的实时监测而设计,在这些环境中,气相色谱/质谱(GC/MS)的性能不佳。为了评估该设备的识别能力、响应时间和定量准确性,使用甲乙酮进行了实验。甲乙酮在许多工厂中广泛使用,其短期暴露极限(STEL)已由美国政府工业卫生学家会议设定。由于在属于本研究关注测量范围的 300 ppm STEL 中,甲乙酮的可离化量已经超过,因此本研究估计了峰位移量而不是峰强度。在包括甲乙酮 STEL 为 300 ppm 的范围内,获得了高精度的校准曲线。实验结果表明,该设备可用于监测工作环境中的化学物质。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/22a9/8825460/8dfdb8f2cc32/indhealth-60-040-g001.jpg

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