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用锦葵叶制备G-CuO纳米颗粒和G-ZnO纳米颗粒,研究它们的抗菌性能,并在无溶剂微波辅助干磨条件下以G-CuO纳米颗粒为催化剂合成双(吲哚基)甲烷化合物。

Preparation of G-CuO NPs and G-ZnO NPs with mallow leaves, investigation of their antibacterial behavior and synthesis of bis(indolyl)methane compounds under solvent-free microwave assisted dry milling conditions using G-CuO NPs as a catalyst.

作者信息

Sulak Mine

机构信息

Department of Mathematics and Science Education, Faculty of Education, Pamukkale University, Denizli Turkey.

出版信息

Turk J Chem. 2021 Oct 19;45(5):1517-1532. doi: 10.3906/kim-2105-31. eCollection 2021.

Abstract

In this study, biogenic copper and zinc oxide nanoparticles (G-ZnONPs and G-CuONPs) were synthesized by the green synthesis method using L. (Millow) leaf extract and the obtained nanoparticles were characterized in detail with UV-Vis, FTIR, SEM, XRD. The antibacterial properties of the synthesized nanoparticles on gram-positive and gram-negative bacteria were investigated and it was found that the nanoparticles had high antimicrobial activity in the results of the experiments. With the obtained G-CuONPs, the synthesis of bis(indolyl)methanes with the "green" one-pot synthesis using microwave was achieved quickly and with high efficiency, and the thermal behavior of the obtained products was investigated.

摘要

在本研究中,采用绿合成法,利用(米洛)叶提取物合成了生物源铜和氧化锌纳米颗粒(G-ZnONPs和G-CuONPs),并通过紫外可见光谱、傅里叶变换红外光谱、扫描电子显微镜、X射线衍射对所得纳米颗粒进行了详细表征。研究了合成纳米颗粒对革兰氏阳性菌和革兰氏阴性菌的抗菌性能,实验结果表明纳米颗粒具有较高的抗菌活性。利用所得的G-CuONPs,通过微波“绿色”一锅法快速高效地实现了双(吲哚基)甲烷的合成,并对所得产物的热行为进行了研究。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7381/8596557/f9c3cdfc70a7/turkjchem-45-1517-fig001.jpg

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