Department of Prosthodontics, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.
Department of Operative Dentistry, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.
Clin Exp Dent Res. 2022 Feb;8(1):287-293. doi: 10.1002/cre2.527. Epub 2022 Jan 11.
This study aimed to evaluate the effect of different concentrations of titanium dioxide (TiO ) and copper oxide (CuO) nanoparticles on the water sorption and solubility of heat-cured polymethyl methacrylate (PMMA).
Fifty disc-shaped specimens (10 × 2 mm) of heat-cured PMMA were prepared and divided into five groups (n = 10) to be modified with 2.5 wt.% or 7.5 wt.% of either TiO or CuO nanoparticles. One group was left unmodified, serving as the control group. Water sorption and solubility were measured by weighing the specimens before and after immersion in distilled water and desiccation. The data were analyzed by using one-way ANOVA and Tukey's post hoc test (α = .05).
The 2.5 wt.% CuO nanoparticles significantly decreased the water sorption (p = .016), but did not change the water solubility (p = .222) compared with the control group. The 7.5 wt.% CuO and both concentration of TiO nanoparticles did not change the water sorption, but significantly increased the solubility of heat-cured PMMA (p ≤ .05).
Adding 2.5 wt.% CuO nanoparticles to heat-cured PMMA decreases the water sorption; although, it has no significant effect on the solubility. Likewise, 2.5 and 7.5 wt.% TiO and 7.5 wt.% CuO do not affect the water sorption, but increase the water solubility of heat-cured PMMA.
Reinforcing the heat-cured PMMA denture base resin materials with the right concentration and type of nanoparticles can decrease the water sorption of resin base materials, and consequently can influence the durability of dentures.
本研究旨在评估不同浓度的二氧化钛(TiO )和氧化铜(CuO)纳米粒子对热固性聚甲基丙烯酸甲酯(PMMA)水吸附和溶解度的影响。
制备了 50 个热固性 PMMA 圆盘状试件(10×2mm),并将其分为 5 组(n=10),分别用 2.5wt.%或 7.5wt.%的 TiO 或 CuO 纳米粒子进行改性。一组不进行改性,作为对照组。通过在蒸馏水和干燥前、后称重试件来测量水吸附和溶解度。数据采用单因素方差分析和 Tukey 事后检验(α=0.05)进行分析。
与对照组相比,2.5wt.%CuO 纳米粒子显著降低了水吸附(p=0.016),但对水溶解度没有影响(p=0.222)。7.5wt.%CuO 和两种浓度的 TiO 纳米粒子均未改变水吸附,但显著增加了热固性 PMMA 的溶解度(p≤0.05)。
向热固性 PMMA 中添加 2.5wt.%CuO 纳米粒子可降低水吸附;然而,对溶解度没有显著影响。同样,2.5 和 7.5wt.%TiO 和 7.5wt.%CuO 不影响水吸附,但增加了热固性 PMMA 的水溶解度。
用正确浓度和类型的纳米粒子增强热固性 PMMA 基托树脂材料可以降低树脂基材料的水吸附,从而影响义齿的耐用性。