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用于从酒糟中回收多酚的纳滤膜系统的实验研究与数学建模

Experimental Study and Mathematical Modeling of a Nanofiltration Membrane System for the Recovery of Polyphenols from Wine Lees.

作者信息

López-Borrell Alexis, López-Pérez María-Fernanda, Cardona Salvador Cayetano, Lora-García Jaime

机构信息

Instituto de Seguridad Industrial, Radiofísica y Medioambiental (ISIRYM), Universitat Politècnica de València (UPV), Plaza Ferrándiz y Carbonell, s/n, 03801 Alcoy, Spain.

出版信息

Membranes (Basel). 2022 Feb 18;12(2):240. doi: 10.3390/membranes12020240.

DOI:10.3390/membranes12020240
PMID:35207161
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8880071/
Abstract

The winemaking process in Spain generates a significant amount of wastes such as wine lees. Currently, the nanofiltration process is a viable technique for the revalorization of compounds from wastes. In this aspect, this technique can be used for the recovery of compounds, such as polyphenols, as well as active principles widely used in industries, such as pharmaceuticals or cosmetics. Polyphenols are found in acceptable amounts in wine lees wastes and it is interesting to study the nanofiltration process viability to recover them. In order to study this possibility, it is necessary to determine the choice of the best membrane to use and the effect of operational parameters such as pressure, temperature, cross-flow rates, and concentration. In addition, it is important to be able to develop a mathematical model that can help in the future design of lees treatment plants. The treatment of red wine lees to concentrate polyphenols has been studied in a laboratory plant using different membranes (RO and NF) at different pressures (4.5, 9.5, and 14.5 bar), different temperatures (293, 303, and 308 K), and two concentrations (2100 and 1100 mg tyrosol eq·L). The results have been encouraging to consider nanofiltration as a viable technique for the treatment and revalorization of this waste. The most suitable membrane has been the NF270, in which 96% rejection rates have been obtained, with a flux of 30 L·h·m. Moreover, in this study, the Spiegler-Kedem model (SKM) was used to calculate mass transfer constants and permeabilities. Suitable adjustments of these parameters were obtained to validate this mathematical model. For this reason, the SKM might be used in future studies to continue in the research work of the treatment of wine lees wastes.

摘要

西班牙的酿酒过程会产生大量废弃物，如酒糟。目前，纳滤工艺是一种使废弃物中的化合物增值的可行技术。在这方面，该技术可用于回收化合物，如多酚，以及制药或化妆品等行业广泛使用的活性成分。酒糟废弃物中含有适量的多酚，研究纳滤工艺回收多酚的可行性很有意义。为了研究这种可能性，有必要确定最佳使用的膜的选择以及压力、温度、错流速率和浓度等操作参数的影响。此外，能够开发一个数学模型以帮助未来酒糟处理厂的设计也很重要。在实验室装置中，使用不同的膜（反渗透和纳滤）、不同压力（4.5、9.5和14.5巴）、不同温度（293、303和308K）以及两种浓度（2100和1100mg酪醇当量·L）对红葡萄酒酒糟进行处理以浓缩多酚。结果令人鼓舞，可将纳滤视为处理和利用这种废弃物的可行技术。最合适的膜是NF270，其截留率达到96%，通量为30L·h·m。此外，在本研究中，使用斯皮格勒-凯德姆模型（SKM）计算传质常数和渗透率。对这些参数进行了适当调整以验证该数学模型。因此，SKM可用于未来的研究，以继续酒糟废弃物处理的研究工作。

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