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从橄榄树枝条中获得的不同热解温度范围的木醋液的化学成分及抗菌活性

Chemical constituents and antimicrobial activity of wood vinegars at different pyrolysis temperature ranges obtained from Olivers branches.

作者信息

Hou Xiaomei, Qiu Ling, Luo Shihai, Kang Kang, Zhu Mingqiang, Yao Yiqing

机构信息

College of Mechanical and Electronic Engineering, Northwest A&F University Yangling 712100 Shaanxi China

Northwest Research Center of Rural Renewable Energy, Exploitation and Utilization of Ministry of Agriculture, Northwest A&F University Yangling 712100 China.

出版信息

RSC Adv. 2018 Dec 6;8(71):40941-40949. doi: 10.1039/c8ra07491g. eCollection 2018 Dec 4.

Abstract

Pyrolysis is a promising approach for converting biomass to solids, liquids, and gases. Herein wood vinegars (WVs) were produced from pyrolysis of Olivers (EUO) branches in different temperature ranges that were labeled as WV and WV The yield, the physicochemical characteristics, the chemical composition, and the antimicrobial activity of the WVs were comprehensively investigated. During the pyrolysis process, as the temperature increased, the yield of the WVs increased firstly and then decreased, and WV achieved the maximum yield of 236.79 g, accounting for 23.26% of the total amount of raw WVs. However, both the lowest pH value (2.39) and the highest total acid content (12.70%) occurred for WV. GC-MS results demonstrated that six components of WVs for WV were phenols, ketones, aldehydes, alcohols, organic acids, and benzenes, while no clear regularity between the contents of each component and the reaction temperature was found. Thereafter, the antimicrobial activity of WVs was tested, and the results showed that the longest inhibition circle diameter of 24.50 mm for was obtained for WV indicating an excellent antibacterial activity; the overall inhibitory effects of WVs on bacteria were superior to those of plant pathogens and fungus. Therefore, WV showed a better antimicrobial activity than that of WV in this study. The result could be a reference for the further utilization of WVs in the field of antimicrobial development.

摘要

热解是一种将生物质转化为固体、液体和气体的有前景的方法。在此,木醋液(WVs)由欧洲油橄榄(EUO)枝条在不同温度范围内热解制备而成,分别标记为WV和WV 。对WVs的产率、理化特性、化学成分及抗菌活性进行了全面研究。在热解过程中,随着温度升高,WVs的产率先增加后降低,WV达到最大产率236.79 g,占原始WVs总量的23.26%。然而,WV的pH值最低(2.39),总酸含量最高(12.70%)。气相色谱 - 质谱(GC - MS)结果表明,WV的WVs的六种成分是酚类、酮类、醛类、醇类、有机酸类和苯类,各成分含量与反应温度之间未发现明显规律。此后,对WVs的抗菌活性进行了测试,结果表明,WV对 的抑菌圈直径最长,为24.50 mm,表明具有优异的抗菌活性;WVs对细菌的总体抑制作用优于对植物病原菌和真菌的抑制作用。因此,在本研究中,WV比WV表现出更好的抗菌活性。该结果可为WVs在抗菌开发领域的进一步利用提供参考。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0191/9091630/0b133a092967/c8ra07491g-f1.jpg

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