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通过绿色创新方法合成具有抗菌活性的FeO@SiO纳米复合材料修饰的Cu(OH)纳米线及其磁行为研究

Synthesis of Cu(OH) nanowires modified by FeO@SiO nanocomposite via green and innovative method with antibacterial activity and investigation of magnetic behaviours.

作者信息

Zare-Bakheir Ensiye, Ahghari Mohammad Reza, Maleki Ali, Ghafuri Hossein

机构信息

Catalysts and Organic Synthesis Research Laboratory, Department of Chemistry, Iran University of Science and Technology, Tehran 16846-13114, Iran.

出版信息

R Soc Open Sci. 2022 Jun 1;9(6):212025. doi: 10.1098/rsos.212025. eCollection 2022 Jun.

DOI:10.1098/rsos.212025
PMID:35706673
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9156904/
Abstract

In this study, green synthesis of modified Cu(OH) nanowires by FeO@SiO core-shell nanospheres was easily performed via chemical reduction. In other words, the direct coating of Cu(OH) on FeO@SiO was successfully realized without the extra complicated procedures. Various concentrations of synthesized nanocomposites were tested on pathogenic and nosocomial bacteria. In this study, the structural information and characterization of FeO@SiO/Cu(OH) nanowires (FSCNWs) were obtained using FE-SEM, FT-IR, EDX and X-ray diffraction. This nanocomposite can effectively kill important infectious bacteria, including , , , and . Studies have shown that FSCNW nanocomposites affect common antibiotic-resistant bacteria. This result confirms the function of FSCNW as an effective, beneficial and environmentally friendly antibacterial agent that can used in a wide range of applications in medicine. FSCNWs can be separated conveniently from bacteria-containing solutions using a magnet. Compared with nanocomposites based on other metals such as silver and gold, the use of FSCNWs in water treatment has been recommended because of the precursor of copper for its low price and less toxicity. In addition to its special properties such as mild reaction conditions, green synthesis methods, admissible magnetic properties, easy separation, high antibacterial activity and beneficial efficiency.

摘要

在本研究中,通过化学还原法可轻松实现利用FeO@SiO核壳纳米球对改性Cu(OH)纳米线进行绿色合成。换句话说,成功实现了在FeO@SiO上直接包覆Cu(OH),而无需额外的复杂程序。对合成的各种浓度的纳米复合材料针对致病性和医院感染细菌进行了测试。在本研究中,利用场发射扫描电子显微镜(FE-SEM)、傅里叶变换红外光谱(FT-IR)、能谱仪(EDX)和X射线衍射获得了FeO@SiO/Cu(OH)纳米线(FSCNWs)的结构信息和表征。这种纳米复合材料能有效杀灭包括……、……、……、……和……在内的重要感染性细菌。研究表明,FSCNW纳米复合材料对常见的耐抗生素细菌有影响。这一结果证实了FSCNW作为一种有效、有益且环保的抗菌剂的功能,可用于医学领域的广泛应用。利用磁铁可方便地从含细菌溶液中分离出FSCNWs。与基于银和金等其他金属的纳米复合材料相比,由于铜前驱体价格低廉且毒性较小,推荐在水处理中使用FSCNWs。此外,它还具有反应条件温和、绿色合成方法、良好的磁性、易于分离、高抗菌活性和有益效果等特殊性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/e289d2355d1e/rsos212025f08.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/5616fd2a479b/rsos212025f09.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/81c1072e9666/rsos212025f01.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/1c53d7c3ee7c/rsos212025f02.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/3edd1a568d05/rsos212025f03.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/657ba861356e/rsos212025f04.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/fb1e8c417c19/rsos212025f05.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/fa317a7cb025/rsos212025f06.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/bb39d96465a6/rsos212025f07.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/e289d2355d1e/rsos212025f08.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/5616fd2a479b/rsos212025f09.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/81c1072e9666/rsos212025f01.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/1c53d7c3ee7c/rsos212025f02.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/3edd1a568d05/rsos212025f03.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/657ba861356e/rsos212025f04.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/fb1e8c417c19/rsos212025f05.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/fa317a7cb025/rsos212025f06.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/bb39d96465a6/rsos212025f07.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b354/9156904/e289d2355d1e/rsos212025f08.jpg

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