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喷雾热解法制备的铁掺杂MoO薄膜的室温氨气传感性能增强

Enhanced Room Temperature Ammonia Gas Sensing Properties of Fe-Doped MoO Thin Films Fabricated Using Nebulizer Spray Pyrolysis.

作者信息

Alkallas Fatemah H, Ben Gouider Trabelsi Amira, Shkir Mohd, AlFaify Salem

机构信息

Department of Physics, College of Science, Princess Nourah bint Abdulrahman University, P.O. Box 84428, Riyadh 11671, Saudi Arabia.

Advanced Functional Materials & Optoelectronic Laboratory (AFMOL), Department of Physics, Faculty of Science, King Khalid University, Abha 61413, Saudi Arabia.

出版信息

Nanomaterials (Basel). 2022 Aug 15;12(16):2797. doi: 10.3390/nano12162797.

Abstract

MoO thin films are fabricated using nebulizer spray pyrolysis technique, which is doped with Fe at various concentrations of 1, 2, 3, and 4% for ammonia gas sensors application at room temperature. X-ray diffraction (XRD) study confirms the growth of the crystal by Fe doping up to 3%, nano rods shape morphology of the thin film samples observed by field emission scanning electron microscope (FESEM), reduction in bandgap is evidenced via UV-VIS spectrophotometer. Gas sensing study is performed using gas analyzing chamber attached with Keithley source meter. Since 3% Fe doped MoO sample displayed nano rods over the film surface which exhibits highest sensitivity of 38,500%, in a short period of raise and decay time 54 and 6 s. Our findings confirms that the 3% Fe doped MoO films suitability for ammonia gas sensing application.

摘要

采用雾化喷雾热解技术制备了MoO薄膜,为用于室温氨气传感器,该薄膜以1%、2%、3%和4%的不同浓度掺杂铁。X射线衍射(XRD)研究证实,铁掺杂量高达3%时晶体生长,通过场发射扫描电子显微镜(FESEM)观察到薄膜样品呈纳米棒形状形态,通过紫外-可见分光光度计证明带隙减小。使用与吉时利源表相连的气体分析室进行气敏研究。由于3%铁掺杂的MoO样品在薄膜表面呈现纳米棒,在54秒和6秒的短上升和衰减时间内显示出38500%的最高灵敏度。我们的研究结果证实了3%铁掺杂的MoO薄膜适用于氨气传感应用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e963/9414738/14d0c3f5377b/nanomaterials-12-02797-g003.jpg

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