Eickhoff Ralf, Antusch Steffen, Baumgärtner Siegfried, Nötzel Dorit, Hanemann Thomas
Institute for Applied Materials, Karlsruhe Institute of Technology, Hermann-von-Helmholtz-Platz 1, D-76344 Eggenstein-Leopoldshafen, Germany.
Department of Microsystems Engineering, University Freiburg, Georges-Koehler-Allee 102,D-79110 Freiburg, Germany.
Materials (Basel). 2022 Sep 16;15(18):6442. doi: 10.3390/ma15186442.
In this work, a holistic approach for the fabrication of dense Ti6Al4V parts via material extrusion methods (MEX), such as fused filament fabrication (FFF) or fused feedstock deposition (FFD), will be presented. With respect to the requirements of the printing process, a comprehensive investigation of the feedstock development will be described. This covers mainly the amount ratio variation of the main binder components LDPE (low-density polyethylene), HDPE (high-density polyethylene), and wax, characterized by shear and oscillation rheology. Solid content of 60 vol% allowed the 3D printing of even more complex small parts in a reproducible manner. In some cases, the pellet-based FFD seems to be superior to the established FFF. After sintering, a density of 96.6% of theory could be achieved, an additional hot isostatic pressing delivered density values better than 99% of theory. The requirements (mechanical properties, carbon, and oxygen content) for the usage of medical implants (following ASTM F2885-17) were partially fulfilled or shortly missed.
在这项工作中,将介绍一种通过材料挤出方法(MEX),如熔融长丝制造(FFF)或熔融原料沉积(FFD)来制造致密Ti6Al4V零件的整体方法。针对打印工艺的要求,将描述对原料开发的全面研究。这主要涵盖了主要粘合剂成分低密度聚乙烯(LDPE)、高密度聚乙烯(HDPE)和蜡的用量比例变化,通过剪切和振荡流变学进行表征。60体积%的固体含量使得以可重复的方式3D打印更复杂的小零件成为可能。在某些情况下,基于颗粒的FFD似乎优于已有的FFF。烧结后,可实现理论密度的96.6%,额外的热等静压可提供优于理论密度99%的值。对于医疗植入物使用(遵循ASTM F2885 - 17)的要求(机械性能、碳和氧含量)部分得到满足或稍有欠缺。