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搅拌摩擦工艺对 AZ31B 镁合金作为生物材料的力学、摩擦学和生物相容性性能的影响:一项初步研究。

The effect of friction stir process on the mechanical, tribological, and biocompatibility properties of AZ31B magnesium alloy as a biomaterial: A pilot study.

机构信息

Department of Mechanical Engineering, Faculty of Engineering, Karadeniz Technical University, Trabzon, Turkey.

Department of Molecular Biology and Genetics, Faculty of Science, Karadeniz Technical University, Trabzon, Turkey.

出版信息

Proc Inst Mech Eng H. 2022 Dec;236(12):1720-1731. doi: 10.1177/09544119221135687. Epub 2022 Nov 8.

Abstract

Recently, AZ31B magnesium alloy has been widely employed in automotive, aerospace, and bio implant industries due to its light-weight and biocompatibility properties. However, the equilibrium of ductility and strength of this material and the negativity brought by its poor wear behavior have limited its versatile use. Friction stir processing (FSP) has been commonly used as severe plastic deformation method for improving mechanical and tribological properties of metal sheets. The effect of this method on the biocompatibility of materials is a matter of curiosity that should be emphasized. So, the present study aims to investigate the effect of friction stir process on the mechanical, tribological, and biocompatibility properties of AZ31B magnesium alloy. It is observed that FSP enhanced the tensile properties of the alloy but decreased its elongation. It was determined that the base material exhibited ductile character on the fracture surface of the specimens, and mixed ductile/brittle fracture was evident with the FSP. In the FSP zone, the hardness value was improved by 17% compared to the base material. Also, the wear performance of the alloy enhanced in ambient air and Simulated Body Fluid (SBF) solution. Wear properties in SBF solution were better due to less adhesive bonds between the friction surfaces. This assessment was supported by SEM images of the wear path and surface of counter bodies. On the other hand, FSPed AZ31B alloy materials with improved strength properties were not cytotoxic for human gingival fibroblasts, and these results may suggest that the materials are safe for clinical uses.

摘要

最近,AZ31B 镁合金由于其轻量和生物相容性的特点,在汽车、航空航天和生物植入体等行业得到了广泛的应用。然而,该材料的延展性和强度的平衡以及较差的耐磨性带来的负面影响限制了其广泛应用。搅拌摩擦加工(FSP)作为一种常用的剧烈塑性变形方法,可用于改善金属板材的力学和摩擦学性能。该方法对材料生物相容性的影响是一个值得关注的问题。因此,本研究旨在研究搅拌摩擦工艺对 AZ31B 镁合金力学、摩擦学和生物相容性的影响。结果表明,FSP 提高了合金的拉伸性能,但降低了其伸长率。确定了基材在试样的断口表面上表现出韧性特征,并且在 FSP 中表现出韧性/脆性混合断裂。在 FSP 区,与基体材料相比,硬度值提高了 17%。此外,在环境空气中和模拟体液(SBF)溶液中,合金的磨损性能得到了提高。在 SBF 溶液中的磨损性能更好,因为摩擦表面之间的粘附结合较少。这一评估得到了摩擦表面磨损路径和表面的 SEM 图像的支持。另一方面,具有增强强度性能的 FSPed AZ31B 合金材料对人牙龈成纤维细胞没有细胞毒性,这些结果可能表明这些材料适用于临床应用。

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