Aykas Didem P
Department of Food Engineering, Faculty of Engineering, Adnan Menderes University, 09100 Aydin, Turkey.
Foods. 2023 Jan 24;12(3):523. doi: 10.3390/foods12030523.
This study aims to predict several quality traits in commercial honey samples simultaneously and to reveal possible honey adulteration using a field-deployable portable infrared spectrometer without any sample preparation. A total of one hundred and forty-seven commercial honey samples were purchased from local and online markets in Turkey and the United States of America (USA), and their soluble solids (°Brix), pH, free acidity, moisture, water activity (aw), glucose, fructose, sucrose, and hydroxymethyl furfural (HMF) contents were determined using reference methods. The HMF ( = 11 samples) and sucrose ( = 21) concentrations were higher than the regulatory limits in some tested samples. The exceeding HMF content may imply temperature abuse during storage and prolonged storing. On the other hand, high sucrose content may indicate possible adulteration with commercial sweeteners. Therefore, soft independent modeling of class analogies (SIMCA) analysis was conducted to reveal this potential sweetener adulteration in the samples, and the SIMCA model was able to identify all the flagged samples. The suggested FT-IR technique may be helpful in regulatory bodies in determining honey authenticity issues as well as assessing the quality characteristics of honey samples in a shorter period and at a lower cost.
本研究旨在同时预测商业蜂蜜样品中的几种品质特性,并使用无需任何样品制备的现场可部署便携式红外光谱仪揭示可能的蜂蜜掺假情况。从土耳其和美利坚合众国(美国)的当地市场和在线市场购买了总共147个商业蜂蜜样品,并使用参考方法测定了它们的可溶性固形物(波美度)、pH值、游离酸度、水分、水分活度(aw)、葡萄糖、果糖、蔗糖和羟甲基糠醛(HMF)含量。在一些测试样品中,HMF( = 11个样品)和蔗糖( = 21个样品)的浓度高于监管限值。HMF含量超标可能意味着储存期间温度过高和储存时间过长。另一方面,高蔗糖含量可能表明可能掺有商业甜味剂。因此,进行了类类比软独立建模(SIMCA)分析以揭示样品中这种潜在的甜味剂掺假情况,并且SIMCA模型能够识别所有标记的样品。所建议的傅里叶变换红外(FT-IR)技术可能有助于监管机构确定蜂蜜的真实性问题,并以更短的时间和更低的成本评估蜂蜜样品的质量特性。