Hydrothermally Grown MoS as an Efficient Electrode Material for the Fabrication of a Resorcinol Sensor.

Recently, the active surface modification of glassy carbon electrodes (GCE) has received much attention for the development of electrochemical sensors. Nanomaterials are widely explored as surface-modifying materials. Herein, we have reported the hydrothermal synthesis of molybdenum disulfide (MoS) and its electro-catalytic properties for the fabrication of a resorcinol sensor. Structural properties such as surface morphology of the prepared MoS was investigated by scanning electron microscopy and phase purity was examined by employing the powder X-ray diffraction technique. The presence of Mo and S elements in the obtained MoS was confirmed by energy-dispersive X-ray spectroscopy. Finally, the active surface of the glassy carbon electrode was modified with MoS. This MoS-modified glassy carbon electrode (MGC) was explored as a potential candidate for the determination of resorcinol. The fabricated MGC showed a good sensitivity of 0.79 µA/µMcm and a detection limit of 1.13 µM for the determination of resorcinol. This fabricated MGC also demonstrated good selectivity, and stability towards the detection of resorcinol.