Wang Si-Qi, Zhao Xi, Ren Xian-Wei, Zhang Zhi-Min, Tian Xue-Dong, He Ya-Yun
School of Aerospace Engineering, North University of China, Taiyuan 030051, China.
Engineering Technology Research Center for Integrated Precision Forming of Shanxi Province, North University of China, Taiyuan 030051, China.
Materials (Basel). 2023 Feb 24;16(5):1880. doi: 10.3390/ma16051880.
In this paper, a hot processing map that takes into the strengthening effect into account is optimized for the Al-10.0Zn-3.0Mg-2.8Cu alloy, mainly considering the crushing and dissolving behavior of the insoluble phase. The hot deformation experiments were performed by compression testing with strain rates ranging from 0.001 to 1 s and the temperature ranging from 380 to 460 °C. The hot processing map was established at the strain of 0.9. It exhibits that the appropriate hot processing region is located at the temperature from 431 to 456 °C and its strain rate is within 0.004-0.108 s. The recrystallization mechanisms and insoluble phase evolution were demonstrated using the real-time EBSD-EDS detection technology for this alloy. It is verified that the work hardening can also be consumed by the coarse insoluble phase refinement with the strain rate increasing from 0.001 to 0.1 s, besides the traditional recovery and recrystallization, but the effect of the insoluble phase crushing was weakened when strain rate increased over 0.1 s. Better refinement of the insoluble phase was around strain rate in 0.1 s, which exhibits adequate dissolving during the solid solution treatment, leading to excellent aging strengthen effects. Finally, the hot processing region was further optimized, so that the strain rate approaches 0.1 s instead of 0.004-0.108 s. This will provide a theoretical support for the subsequent deformation of the Al-10.0Zn-3.0Mg-2.8Cu alloy and its' engineering application in aerospace, defense and military fields.
本文针对Al-10.0Zn-3.0Mg-2.8Cu合金,考虑强化效果优化了热加工图,主要考虑了不溶相的破碎和溶解行为。通过压缩试验进行热变形实验,应变速率范围为0.001至1 s,温度范围为380至460°C。在应变为0.9时建立了热加工图。结果表明,合适的热加工区域位于431至456°C,应变速率在0.004 - 0.108 s范围内。利用该合金的实时EBSD-EDS检测技术研究了再结晶机制和不溶相演变。结果表明,除了传统的回复和再结晶外,随着应变速率从0.001增加到0.1 s,加工硬化也可被粗大不溶相的细化所消耗,但当应变速率超过0.1 s时,不溶相破碎的效果减弱。在应变速率为0.1 s左右时,不溶相得到更好的细化,在固溶处理过程中表现出充分的溶解,从而产生优异的时效强化效果。最后,对热加工区域进行了进一步优化,使应变速率接近0.1 s而不是0.004 - 0.108 s。这将为Al-10.0Zn-3.0Mg-2.8Cu合金的后续变形及其在航空航天、国防和军事领域的工程应用提供理论支持。