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通过专用 V 形传感器进行在线 NMR。

Inline NMR via a Dedicated V-Shaped Sensor.

机构信息

Institute of Mechanical Process Engineering and Mechanics, Karlsruhe Institute of Technology, 76131 Karlsruhe, Germany.

Engler-Bunte-Institut, Chair of Water Chemistry and Water Technology, Karlsruhe Institute of Technology, 76131 Karlsruhe, Germany.

出版信息

Sensors (Basel). 2023 Feb 21;23(5):2388. doi: 10.3390/s23052388.

Abstract

Process monitoring and control require dedicated and reliable measures which reflect the status of the process under investigation. Although nuclear magnetic resonance is known to be a versatile analytical technique, it is only seldomly found in process monitoring. Single-sided nuclear magnetic resonance is one well known approach for being applied in process monitoring. The dedicated V-sensor is a recent approach that allows the inline investigation of materials in a pipe non-destructively and non-invasively. An open geometry of the radiofrequency unit is realized using a tailored coil, enabling the sensor to be applied for manifold mobile applications in in-line process monitoring. Stationary liquids were measured, and their properties were integrally quantified as the basis for successful process monitoring. The sensor, in its inline version, is presented along with its characteristics. An exemplary field of application is battery production in terms of anode slurries; thus, the first results on graphite slurries will demonstrate the added value of the sensor in process monitoring.

摘要

过程监测和控制需要专用且可靠的测量方法,以反映被研究过程的状态。尽管核磁共振已被公认为是一种多功能的分析技术,但它在过程监测中却很少使用。单面核磁共振是一种常用于过程监测的方法。专用 V 传感器是一种最近的方法,它允许对管道中的材料进行非破坏性和非侵入式的在线研究。使用定制线圈实现了射频单元的开放式结构,从而使传感器能够应用于在线过程监测中的多种移动应用。对静止液体进行了测量,并对其性质进行了整体量化,以此作为成功进行过程监测的基础。该传感器的在线版本及其特点将一并呈现。以阳极浆料为例,电池生产是一个应用领域;因此,石墨浆料的首批结果将展示该传感器在过程监测中的附加价值。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1d39/10007489/7499802fa7b8/sensors-23-02388-g001.jpg

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