Department of Chemical and Biochemical Engineering, Faculty of Chemical Engineering and Biotechnologies, University "Politehnica" of Bucharest, 1-7 Polizu Street, 011061 Bucharest, Romania.
Department of Organic Chemistry "Costin Neniţescu", Faculty of Chemical Engineering and Biotechnologies, University "Politehnica" of Bucharest, 1-7 Polizu Street, 011061 Bucharest, Romania.
Molecules. 2023 Mar 8;28(6):2486. doi: 10.3390/molecules28062486.
Ultrasound-assisted extraction (UAE) was applied to extract oil from blackberry (BB) seeds. The effect of UAE conditions on oil recovery and quality was investigated. Favorable experimental conditions (ultrasound intensity (UI), extraction temperature, and time) were investigated using response surface methodology (RSM). A Box-Behnken design was used to predict optimized conditions for BB seed oil extraction. These conditions were as follows: 13.77 W/cm UI, 45 °C extraction temperature, and 15 min extraction time. The experimental value obtained for extraction efficiency under optimal conditions was 87 ± 0.34%, in good agreement with the optimized predicted value. UAE does not affect the oil composition and confers higher antioxidant values in BB seed oil in comparison with Soxhlet extraction.
超声辅助提取(UAE)被应用于从黑莓(BB)种子中提取油。研究了 UAE 条件对油回收率和质量的影响。使用响应面法(RSM)研究了有利的实验条件(超声强度(UI)、提取温度和时间)。采用 Box-Behnken 设计预测了 BB 籽油提取的最佳条件。这些条件如下:UI 为 13.77 W/cm,提取温度为 45°C,提取时间为 15 分钟。在最佳条件下,提取效率的实验值为 87 ± 0.34%,与优化预测值吻合良好。与索氏提取相比,UAE 不影响油的组成,并赋予 BB 籽油更高的抗氧化值。