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蜂蜜中磺胺噻唑残留的快速定量薄层色谱筛选方法

Rapid quantitative thin layer chromatographic screening procedure for sulfathiazole residues in honey.

作者信息

Neidert E, Baraniak Z, Sauvé A

出版信息

J Assoc Off Anal Chem. 1986 Jul-Aug;69(4):641-3.

PMID:3745091
Abstract

A procedure is presented for the quantitative determination of sulfathiazole residues in honey. Induced fluorescence of sulfathiazole is measured by fluorescent scanning densitometry; sulfaquinoxaline is added as an internal standard for quantitation. Recovery is greater than 98% and results are linear over the range 0.05-0.60 mg/kg. The detection limit, CL (k = 3), is 0.02. The procedure allows a single analyst to process 50-60 samples/day.

摘要

本文介绍了一种定量测定蜂蜜中磺胺噻唑残留量的方法。通过荧光扫描密度计测量磺胺噻唑的诱导荧光;添加磺胺喹恶啉作为内标进行定量。回收率大于98%,结果在0.05 - 0.60 mg/kg范围内呈线性。检测限CL(k = 3)为0.02。该方法允许一名分析人员每天处理50 - 60个样品。

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