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高速烧结对5 mol%氧化钇稳定的多层氧化锆光学性能、微观结构和相分布的影响

Effect of High-Speed Sintering on the Optical Properties, Microstructure, and Phase Distribution of Multilayered Zirconia Stabilized with 5 mol% Yttria.

作者信息

Cho Mi-Hyang, Seol Hyo-Joung

机构信息

Department of Dental Lab, Wonkwang Health Science University, Iksan-si 54538, Republic of Korea.

Department of Dental Materials, Dental and Life Science Institute, School of Dentistry, Pusan National University, Yangsan-si 50612, Republic of Korea.

出版信息

Materials (Basel). 2023 Aug 10;16(16):5570. doi: 10.3390/ma16165570.

Abstract

As dental 5 mol% yttria-stabilized (5Y-) zirconia demand high esthetics, it is necessary to clarify how the optical properties are affected by high-speed sintering, which is not yet fully understood. Our study aimed to investigate the effect of high-speed sintering on the translucency and opalescence parameters (TP and OP, respectively), as well as their related microstructure and phase distribution, using two types of multilayered 5Y-zirconia. Multilayered 5Y-zirconia (Cercon xt ML, Lava Esthetic) were cut layer-by-layer, followed by conventional and high-speed sintering. The TP and OP values were subsequently obtained using a spectrophotometer, and field emission scanning electron microscopy images were used to analyze the average grain size. The phase fractions were analyzed using X-ray diffraction. Regardless of the zirconia type, the TP was slightly lowered by high-speed sintering in all the layers except the dentin layer (DL) for Lava Esthetic ( < 0.05). The OP decreased by high-speed sintering in the DL for Cercon xt ML and in all the layers for Lava Esthetic ( < 0.05). The decrease in translucency after high-speed sintering was attributed to a decrease in the yttria-rich '-phase with low tetragonality, along with an increase in the yttria-lean -phase with high tetragonality.

摘要

由于牙科用5摩尔%氧化钇稳定(5Y-)氧化锆需要高美学性能,因此有必要阐明高速烧结如何影响其光学性能,而目前对此尚未完全了解。我们的研究旨在使用两种类型的多层5Y-氧化锆,研究高速烧结对透明度和乳光参数(分别为TP和OP)及其相关微观结构和相分布的影响。将多层5Y-氧化锆(Cercon xt ML、Lava Esthetic)逐层切割,然后进行常规烧结和高速烧结。随后使用分光光度计获得TP和OP值,并使用场发射扫描电子显微镜图像分析平均晶粒尺寸。使用X射线衍射分析相分数。无论氧化锆类型如何,对于Lava Esthetic,除牙本质层(DL)外,所有层的高速烧结都会使TP略有降低(<0.05)。对于Cercon xt ML,DL中的OP因高速烧结而降低,对于Lava Esthetic,所有层中的OP均因高速烧结而降低(<0.05)。高速烧结后透明度的降低归因于四方度低的富钇'-相减少,以及四方度高的贫钇-相增加。

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