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刺云实胶作为壁材的初步评估:不同干燥方法的物理化学、结构、热学及流变学分析

Preliminary Assessment of Tara Gum as a Wall Material: Physicochemical, Structural, Thermal, and Rheological Analyses of Different Drying Methods.

作者信息

Moscoso-Moscoso Elibet, Ligarda-Samanez Carlos A, Choque-Quispe David, Huamán-Carrión Mary L, Arévalo-Quijano José C, De la Cruz Germán, Luciano-Alipio Rober, Calsina Ponce Wilber Cesar, Sucari-León Reynaldo, Quispe-Quezada Uriel R, Calderón Huamaní Dante Fermín

机构信息

Nutraceuticals and Biomaterials Research Group, Universidad Nacional José María Arguedas, Andahuaylas 03701, Peru.

Research Group in the Development of Advanced Materials for Water and Food Treatment, Universidad Nacional José María Arguedas, Andahuaylas 03701, Peru.

出版信息

Polymers (Basel). 2024 Mar 19;16(6):838. doi: 10.3390/polym16060838.

DOI:10.3390/polym16060838
PMID:38543443
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10975910/
Abstract

Tara gum, a natural biopolymer extracted from seeds, was investigated in this study. Wall materials were produced using spray drying, forced convection, and vacuum oven drying. In addition, a commercial sample obtained through mechanical methods and direct milling was used as a reference. The gums exhibited low moisture content (8.63% to 12.55%), water activity (0.37 to 0.41), bulk density (0.43 to 0.76 g/mL), and hygroscopicity (10.51% to 11.42%). This allows adequate physical and microbiological stability during storage. Polydisperse particles were obtained, ranging in size from 3.46 µm to 139.60 µm. Fourier transform infrared spectroscopy characterisation confirmed the polysaccharide nature of tara gum, primarily composed of galactomannans. Among the drying methods, spray drying produced the gum with the best physicochemical characteristics, including higher lightness, moderate stability, smaller particle size, and high glass transition temperature (141.69 °C). Regarding rheological properties, it demonstrated a non-Newtonian pseudoplastic behaviour that the power law could accurately describe. The apparent viscosity of the aqueous dispersions of the gum decreased with increasing temperature. In summary, the results establish the potential of tara gum as a wall material applicable in the food and pharmaceutical industries.

摘要

塔拉胶是一种从种子中提取的天然生物聚合物,本研究对其进行了调查。采用喷雾干燥、强制对流和真空烘箱干燥的方法制备壁材。此外,通过机械方法和直接研磨获得的商业样品用作参考。这些胶表现出低水分含量(8.63%至12.55%)、水分活度(0.37至0.41)、堆积密度(0.43至0.76 g/mL)和吸湿性(10.51%至11.42%)。这使得在储存期间具有足够的物理和微生物稳定性。获得了多分散颗粒,粒径范围为3.46 µm至139.60 µm。傅里叶变换红外光谱表征证实了塔拉胶的多糖性质,主要由半乳甘露聚糖组成。在干燥方法中,喷雾干燥制备的胶具有最佳的物理化学特性,包括更高的亮度、适度的稳定性、更小的粒径和高玻璃化转变温度(141.69°C)。关于流变学性质,它表现出非牛顿假塑性行为,幂律可以准确描述。胶的水分散体的表观粘度随温度升高而降低。总之,结果证实了塔拉胶作为一种适用于食品和制药行业的壁材的潜力。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/2f2916d63681/polymers-16-00838-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/c19a0d100571/polymers-16-00838-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/c55a29c4bf1b/polymers-16-00838-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/cb87a1739c3a/polymers-16-00838-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/beed3f043869/polymers-16-00838-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/d2a9bff9be18/polymers-16-00838-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/4810ded91d09/polymers-16-00838-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/f03277ca4907/polymers-16-00838-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/2f2916d63681/polymers-16-00838-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/c19a0d100571/polymers-16-00838-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/c55a29c4bf1b/polymers-16-00838-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/cb87a1739c3a/polymers-16-00838-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/beed3f043869/polymers-16-00838-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/d2a9bff9be18/polymers-16-00838-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/4810ded91d09/polymers-16-00838-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/f03277ca4907/polymers-16-00838-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9eb/10975910/2f2916d63681/polymers-16-00838-g008.jpg

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