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储存条件对牙科树脂基复合材料断裂可靠性和物理性能的影响。

Impact of storage conditions on the fracture reliability and physical properties of a dental resin-based composite.

作者信息

Al-Zain Afnan Omar, Piva Evandro, Pimentel Alice Hammes, Duarte Camila Gonçalves, Valente Lisia Lorea, Isolan Cristina Pereira, Münchow Eliseu Aldrighi

机构信息

King Abdulaziz University, Faculty of Dentistry, Restorative Dentistry Department, Jeddah, Saudi Arabia.

Universidade Federal de Pelotas - UFPel, Developmental and Control Center of Biomaterials, Department of Restorative Dentistry, Pelotas, RS. Brazil.

出版信息

Braz Oral Res. 2024 Jul 12;38:e062. doi: 10.1590/1807-3107bor-2024.vol38.0062. eCollection 2024.

Abstract

This study investigated the impact of 'storage condition' and 'period of storage' on selected physico-mechanical properties and fracture reliability of a resin-based composite (RBC). Specimens, prepared from a nanofilled RBC (Filtek Z350 XT; 3M ESPE), underwent tests for degree of conversion (DC), flexural strength (σ), flexural modulus (E), and hardness. The specimens were initially grouped into dry storage at 37°C or wet storage in distilled water at 37°C. Subsequently, they were further divided into four subgroups based on the period of storage: 6, 24, 72, or 168 hours. Specimens tested immediately after preparation served as control. Data analysis employed two-way ANOVA and Weibull analysis (α = 5%). Compared to the control, an increase in DC was observed only after 72 hours of dry storage; σ showed higher values after both dry and wet storage, regardless of the storage period (except for the group wet-stored for 168 hours); E increased with dry storage for at least 24 hours or wet storage for 72 hours; and hardness increased after dry storage for at least 24 hours or wet storage for up to 72 hours. The Weibull modulus remained unchanged under any of the distinct storage conditions. Dry storage resulted in greater characteristic strength than the control, whereas wet storage contributed to higher strength values only at shorter periods (up to 24 hours). Overall, the inherent properties of RBCs with a similar composition to that tested in this study may change with varying storage conditions and periods.

摘要

本研究调查了“储存条件”和“储存时间”对一种树脂基复合材料(RBC)选定的物理机械性能及断裂可靠性的影响。由纳米填充RBC(Filtek Z350 XT;3M ESPE)制备的试样,进行了转化率(DC)、弯曲强度(σ)、弯曲模量(E)和硬度测试。试样最初分为在37°C下干燥储存或在37°C的蒸馏水中湿储存两组。随后,根据储存时间将它们进一步分为四个亚组:6、24、72或168小时。制备后立即测试的试样作为对照。数据分析采用双向方差分析和威布尔分析(α = 5%)。与对照组相比,仅在干燥储存72小时后观察到DC增加;无论储存时间如何(湿储存168小时的组除外),干燥和湿储存后σ均显示出较高的值;干燥储存至少24小时或湿储存72小时后E增加;干燥储存至少24小时或湿储存长达72小时后硬度增加。在任何不同的储存条件下,威布尔模量均保持不变。干燥储存导致特征强度高于对照组,而湿储存仅在较短时间(长达24小时)内导致强度值更高。总体而言,与本研究中测试的具有相似组成的RBC的固有性能可能会随储存条件和时间的变化而改变。

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