Viciana Eduardo, Martínez-Lao Juan Antonio, López-Lao Emilio, Fernández Ignacio, Arrabal-Campos Francisco Manuel
Department of Engineering, Research Centre CIMEDES, Escuela Superior de Ingeniería, University of Almería, 04120 Almeria, Spain.
Department of Chemistry and Physics, Research Centre CIAIMBITAL, University of Almería, 04120 Almeria, Spain.
Sensors (Basel). 2024 Aug 27;24(17):5537. doi: 10.3390/s24175537.
Today, it is difficult to have a high-field nuclear magnetic resonance (NMR) device due to the high cost of its acquisition and maintenance. These high-end machines require significant space and specialist personnel for operation and offer exceptional quality in the acquisition, processing, and other advanced functions associated with detected signals. However, alternative devices are low-field nuclear magnetic resonance devices. They benefit from the elimination of high-tech components that generate static magnetic fields and advanced instruments. Instead, they used magnetic fields induced by ordinary conductors. Another category of spectrometers uses the Earth's magnetic field, which is simple and economical but limited in use. These devices are called Earth-Field Nuclear Magnetic Resonance (EFNMR) devices. This device is ideal for educational purposes, especially for engineers and those who study nuclear magnetic resonance, such as chemistry or other experimental sciences. Students can observe their internal workings and conduct experiments that complement their education without worrying about damaging equipment. This article provides a detailed explanation of the design and construction of electrical technology devices for the excitation of atomic spin resonance using Earth's magnetic fields. It covers all necessary stages, from research to analysis, including simulation, assembly, construction of each component, and the development of comprehensive software for spectrometer control.
如今,由于购置和维护成本高昂,拥有一台高场核磁共振(NMR)设备并非易事。这些高端仪器需要大量空间且需专业人员操作,在采集、处理以及与检测信号相关的其他高级功能方面具备卓越品质。然而,替代设备是低场核磁共振设备。它们受益于去除了产生静磁场的高科技部件和先进仪器。相反,它们使用普通导体感应的磁场。另一类光谱仪利用地磁场,这种方式简单且经济,但使用受限。这些设备被称为地场核磁共振(EFNMR)设备。该设备非常适合用于教育目的,尤其适用于工程师以及研究核磁共振的人员,如化学或其他实验科学领域的人员。学生可以观察其内部工作原理并进行补充其学业的实验,而无需担心损坏设备。本文详细解释了利用地磁场激发原子自旋共振的电气技术设备的设计与构造。它涵盖了从研究到分析的所有必要阶段,包括模拟、组装、各部件的构建以及用于光谱仪控制的综合软件的开发。