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揭示大量AlRE相增强的高模量Mg-15Gd-8Y-6Al-0.3Mn合金压缩过程中的微观结构特征。

Unveiling the Microstructural Features during Compression of a High-Modulus Mg-15Gd-8Y-6Al-0.3Mn Alloy Reinforced by a Large Volume of AlRE Phases.

作者信息

Feng Xuhui, Wang Xiaojun, Xu Chao, Shi Hailong, Li Xuejian, Hu Xiaoshi, Lu Zhen, Fan Guohua

机构信息

State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001, China.

Center for Analysis and Measurement, Harbin Institute of Technology, Harbin 150001, China.

出版信息

Materials (Basel). 2024 Sep 29;17(19):4784. doi: 10.3390/ma17194784.

DOI:10.3390/ma17194784
PMID:39410355
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11477671/
Abstract

Magnesium alloys with a high volume fraction of secondary phases exhibit inferior formability. Therefore, investigating their thermal deformation characteristics is critical for optimizing thermal processing techniques. In this work, isothermal compression experiments were performed on a Mg-15Gd-8Y-6Al-0.3Mn alloy with an elastic modulus of 51.3 GPa with a substantial volume of aluminum-rare earth (AlRE) phases. The rheological behavior and microstructural evolution of the material were systematically investigated at varying temperatures (350-500 °C) and strain rates (0.001-1.000 s). The calculated thermal processing diagram indicates that the unstable region gradually enlarges with increased strain, and all unstable regions appear within the high-strain-rate, low-temperature domain. The ideal thermal processing range of the alloy is 350-500 °C at strain rates ranging from 0.001 to 0.016 s. Particle-stimulated nucleation and discontinuous dynamic recrystallization are both verified to be responsible for the recrystallized microstructure of the alloy. The recrystallized grains exhibit a relatively random crystallographic orientation. As recrystallization proceeds, the texture gradually transitions from a typical [0001] texture in the compression direction to a random texture accompanied by decreased texture intensity. This work sheds new light on the thermo-mechanical processing of high-modulus Mg alloys, which could help design suitable processing techniques for related materials.

摘要

具有高体积分数第二相的镁合金表现出较差的可加工性。因此,研究它们的热变形特性对于优化热加工工艺至关重要。在这项工作中,对一种弹性模量为51.3 GPa且含有大量铝稀土(AlRE)相的Mg-15Gd-8Y-6Al-0.3Mn合金进行了等温压缩实验。系统地研究了该材料在不同温度(350 - 500 °C)和应变速率(0.001 - 1.000 s)下的流变行为和微观结构演变。计算得到的热加工图表明,不稳定区域随着应变增加而逐渐扩大,并且所有不稳定区域都出现在高应变速率、低温区域内。该合金的理想热加工范围是在应变速率为0.001至0.016 s时温度为350 - 500 °C。颗粒激发形核和不连续动态再结晶都被证实是该合金再结晶微观结构的成因。再结晶晶粒表现出相对随机的晶体取向。随着再结晶的进行,织构逐渐从压缩方向上典型的[0001]织构转变为随机织构,同时织构强度降低。这项工作为高模量镁合金的热机械加工提供了新的见解,这有助于为相关材料设计合适的加工工艺。

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本文引用的文献

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Effect of LPSO and SFs on microstructure evolution and mechanical properties of Mg-Gd-Y-Zn-Zr alloy.LPSO 和 SFs 对 Mg-Gd-Y-Zn-Zr 合金组织演变和力学性能的影响。
Sci Rep. 2017 Jan 30;7:40846. doi: 10.1038/srep40846.