Ueta Ikuo, Nakagami Koki, Saito Yoshihiro
Department of Applied Chemistry, University of Yamanashi, 4-3-11 Takeda, Kofu, 400-8511, Japan.
Department of Applied Chemistry and Life Science, Toyohashi University of Technology, 1-1 Hibarigaoka, Tempaku, Toyohashi, 441-8580, Japan.
Anal Sci. 2025 May;41(5):505-510. doi: 10.1007/s44211-025-00729-5. Epub 2025 Feb 26.
Solid-phase extraction (SPE) is a sample preparation technique typically used for purifying target analytes in liquid samples prior to instrumental analysis, such as chromatographic analysis. Typical SPE device consists of packing particulate adsorbent into a glass or plastic cartridge. In the sample preparation process, the target analytes are extracted onto the adsorbent by loading the liquid sample into the SPE cartridge and separated from other contaminants. Then, the extracted compounds are eluted by the organic solvent. This article summarizes the SPE devices designed for extracting volatile organic compounds in gaseous samples. In these SPE devices, the extracted analytes are eluted by simply passing the desorption solvent. The devices can be reused after drying the adsorbent.
固相萃取(SPE)是一种样品制备技术,通常用于在仪器分析(如色谱分析)之前净化液体样品中的目标分析物。典型的SPE装置是将颗粒状吸附剂填充到玻璃或塑料柱中。在样品制备过程中,通过将液体样品加载到SPE柱中,目标分析物被萃取到吸附剂上,并与其他污染物分离。然后,用有机溶剂洗脱萃取的化合物。本文总结了用于萃取气态样品中挥发性有机化合物的SPE装置。在这些SPE装置中,通过简单地使解吸溶剂通过来洗脱萃取的分析物。干燥吸附剂后,这些装置可以重复使用。