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作为草药制剂特征的核磁共振氢谱。

1H NMR spectra as a characteristic of herbal preparations.

作者信息

Thakur Rajendra Singh, Jayakrishnan Neelima, Das Arun Kumar

机构信息

Analytical and Environmental Science Division and Centralized Instrument Facility, CSIR-Central Salt and Marine Chemicals Research Institute (CSIR-CSMCRI), Council of Scientific & Industrial Research (CSIR), Gijubhai Badheka Marg, Bhavnagar, Gujarat 364002 India.

Academy of Scientific and Innovative Research (AcSIR), Ghaziabad, 201002 India.

出版信息

J Food Sci Technol. 2025 Jul;62(7):1338-1349. doi: 10.1007/s13197-024-06107-9. Epub 2024 Oct 17.


DOI:10.1007/s13197-024-06107-9
PMID:40538963
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12173972/
Abstract

UNLABELLED: This study attempts the application of 1H NMR spectra as a characteristic of commercial herbal preparations. 1H NMR spectra of four herbal preparations having the same composition from different manufacturers were compared. 1H NMR spectra of three herbal preparations having different compositions from commercial sources were also examined. 2D NMR TOCSY spectra of the same preparations were also presented for correlation of 1H NMR spectra with herbal composition. Average and standard deviation were derived from 1H NMR spectra of four herbal preparations of the same composition (Triphala) as a comparative analytical method. GRAPHICAL ABSTRACT: Composition of herbal preparation is correlated with 1H NMR spectra. SUPPLEMENTARY INFORMATION: The online version contains supplementary material available at 10.1007/s13197-024-06107-9.

摘要

未标注:本研究尝试将1H NMR光谱应用于商业草药制剂的特征分析。比较了来自不同制造商的四种成分相同的草药制剂的1H NMR光谱。还研究了来自商业来源的三种成分不同的草药制剂的1H NMR光谱。同时给出了相同制剂的二维NMR TOCSY光谱,以关联1H NMR光谱与草药成分。作为一种比较分析方法,从四种成分相同(三果木)的草药制剂的1H NMR光谱中得出平均值和标准差。 图形摘要:草药制剂的成分与1H NMR光谱相关。 补充信息:在线版本包含可在10.1007/s13197-024-06107-9获取的补充材料。

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本文引用的文献

[1]
Triphala inhibits alpha-synuclein fibrillization and their interaction study by NMR provides insights into the self-association of the protein.

RSC Adv. 2019-9-10

[2]
Method for quick DNA barcode reference library construction.

Ecol Evol. 2021-8-4

[3]
Removal of Paramagnetic Ions Prior to Analysis of Organic Reactions in Aqueous Solutions by NMR Spectroscopy.

ACS Omega. 2021-5-28

[4]
Regulatory landscape of dietary supplements and herbal medicines from a global perspective.

Regul Toxicol Pharmacol. 2020-7

[5]
Herbal Medicine Classification: Policy Recommendations.

Front Med (Lausanne). 2020-2-11

[6]
Temperature dependence of NMR chemical shifts: Tracking and statistical analysis.

Protein Sci. 2019-11-26

[7]
NMR Spectroscopy for Metabolomics Research.

Metabolites. 2019-6-27

[8]
International Comparison of Five Herbal Medicine Registration Systems to Inform Regulation Development: United Kingdom, Germany, United States of America, United Arab Emirates and Kingdom of Bahrain.

Pharmaceut Med. 2018

[9]
Challenges in integrating component level technology and system level information from Ayurveda: Insights from NMR phytometabolomics and anti-HIV potential of select Ayurvedic medicinal plants.

J Ayurveda Integr Med. 2019

[10]
Current and Future Perspectives on the Structural Identification of Small Molecules in Biological Systems.

Metabolites. 2016-12-15

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