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甲基丙烯酸酯基和有机陶瓷基直接复合树脂与间接CAD/CAM复合树脂块的表面粗糙度和颜色变化

Surface roughness and color change of methacrylate and ormocer-based direct composite versus indirect CAD/CAM composite blocks.

作者信息

Saleh Somaya Ali, Hashem Danya

机构信息

Department of Operative Dentistry, Faculty of Dentistry, Ain Shams University, Cairo, Egypt.

Department of Restorative Dental Science, College of Dentistry, Taibah University, Madinah, Saudi Arabia.

出版信息

Saudi Dent J. 2024 Dec;36(12):1559-1565. doi: 10.1016/j.sdentj.2024.11.002. Epub 2024 Nov 16.

Abstract

OBJECTIVES

To assess the color stability and surface roughness of resin-free and resin-based nanohybrid composites after immersion in various staining media

METHODS

A resin-free ormocer composite, Admira fusion (Voco, Germany), and a methacrylate resin composite, Grandio (Voco, Germany), were used for direct composite restorations with 30 discs per material formed using a Split Teflon mold (10 mm × 2 mm). Grandio Bloc (Voco, Germany) universal indirect CAD/CAM block specimens (n = 30) were sliced to a thickness of 2 mm with a precision saw. Each material was divided into 3 groups (n = 10 each) based on the immersion solution. Specimens were soaked in coffee (Turkish coffee, Baja, Saudi Arabia), cola (Coca-Cola Co., USA), and artificial saliva. Color was evaluated before staining and after 30 days of staining using a spectrophotometer. Color change (ΔE*) was measured using the system of CIE Lab*. Surface roughness was determined using a stylus profilometer and represented using Atomic Force Microscopy before and after immersion in the staining solutions.

RESULTS

After immersion in the staining solutions for 30 days, the color values of all the composites changed. Group A (coffee) had the greatest effect (ΔE > 5), and indirect Grandio blocs caused the greatest color change. The surface roughness values increased, particularly in group B (Coca-Cola), for all the tested materials after 30 days. Direct Grandio had a significantly higher roughness than the other materials (p < 0.001).

CONCLUSION

Immersion in coffee resulted in considerable color change, while immersion in cola had the greatest negative impact on surface roughness in all tested restorative materials. The nanohybrid ormocer did not provide better surface integrity than conventional methacrylate-based nanohybrid composites.

摘要

目的

评估无树脂和树脂基纳米混合复合材料在浸入各种染色介质后的颜色稳定性和表面粗糙度。

方法

使用无树脂的有机陶瓷复合材料Admira fusion(德国Voco公司)和甲基丙烯酸酯树脂复合材料Grandio(德国Voco公司)进行直接复合修复,每种材料用分体式聚四氟乙烯模具(10毫米×2毫米)制作30个圆盘。将德国Voco公司的Grandio Bloc通用间接CAD/CAM块状试件(n = 30)用精密锯切成2毫米厚。根据浸泡溶液将每种材料分为3组(每组n = 10)。试件分别浸泡在咖啡(土耳其咖啡,沙特阿拉伯巴哈)、可乐(美国可口可乐公司)和人工唾液中。在染色前和染色30天后使用分光光度计评估颜色。使用CIE Lab系统测量颜色变化(ΔE)。在浸入染色溶液前后,使用触针轮廓仪测定表面粗糙度,并通过原子力显微镜表示。

结果

在染色溶液中浸泡30天后,所有复合材料的颜色值均发生变化。A组(咖啡)的影响最大(ΔE > 5),间接Grandio块引起的颜色变化最大。30天后,所有测试材料的表面粗糙度值均增加,尤其是B组(可乐)。直接使用的Grandio的粗糙度明显高于其他材料(p < 0.001)。

结论

浸入咖啡会导致显著的颜色变化,而浸入可乐对所有测试修复材料的表面粗糙度的负面影响最大。纳米混合有机陶瓷材料在表面完整性方面并不比传统的甲基丙烯酸酯基纳米混合复合材料更好。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f837/11976155/7b6ba1791aac/gr1.jpg

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