[通过薄层层析板直接测量法以1-二甲基氨基萘-5-磺酰氯荧光法测定血浆中的反苯环丙胺（作者译）]
[Fluorimetric determination of tranylcypromine in plasma as its 1-dimethylamino-naphthaline-5-sulfonic acid chloride by direct measurement of TLC-plates (author's transl)].
作者信息
Lang A, Geissler H E, Mutschler E
出版信息
Arzneimittelforschung. 1978;28(4):575-7.
PMID:581930
Abstract
A fluorimetric method for analysis of tranylcypromine from plasma is described. After extraction from plasma tranylcypromine reacts with 1-dimethylamino-naphthaline-5-sulfonic acid chloride (DANS-Cl) in order to form the highly fluorescent DANS-tranylcypromine. After chromatographic separation on silicagel plates quantitation is achieved by in situ fluorescence determination. The recovery of tranylcypromine from plasma is 64% with a coefficient of variance of about +/- 6%.
摘要
本文描述了一种用于分析血浆中反苯环丙胺的荧光分析法。从血浆中提取后，反苯环丙胺与1-二甲基氨基萘-5-磺酰氯（DANS-Cl）反应，以形成高荧光的DANS-反苯环丙胺。在硅胶板上进行色谱分离后，通过原位荧光测定进行定量。血浆中反苯环丙胺的回收率为64%，变异系数约为±6%。
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