Roulet J F, Söderholm K J, Longmate J
Department of Operative Dentistry and Endodontics North, Freie Universität Berlin, Germany.
J Dent Res. 1995 Jan;74(1):381-7. doi: 10.1177/00220345950740011501.
During the past few years, the interest in using ceramic inlays and veneers has increased. New materials and methods have been introduced to bond these restorations to resinous materials. Since our knowledge of how to optimize such bonding is limited, the objective of this study was to test the hypothesis that various surface treatment variables and combinations of these variables affect the strength of the ceramic/composite interphase of ceramic inlays differently. The influences of material composition, surface-roughening method, silane treatment, silane heat treatment, and storage condition on bond strength were investigated. Three ceramics (Dicor, Mirage, Vitabloc), three surface-roughening methods (etching, sandblasting, grinding), three silane treatments (gamma-methacryloxypropyltrimethoxysilane [MPS], MPS+paratoluidine, vinyltrichlorosilane), two heat treatments (20 degrees C for 60 s, 100 degrees C for 60 s), and two storage conditions (24-hour dry, one yr in water at 37 degrees C) were studied. For each of the 108 combinations, five specimens were tested. Ceramic cylinders were treated according to group assignment and bonded to blocks of the same ceramic material with a dual-cured resin. The shear bond strength was determined, and the experimental factors were evaluated by analysis of variance. The results showed that surface-roughening method had the strongest effect on bond strength, while ceramic selection had the least significant effect. Of the surface-roughening methods, etching was associated with higher bond strength values than either sandblasting or grinding.(ABSTRACT TRUNCATED AT 250 WORDS)
在过去几年中,使用陶瓷嵌体和贴面的兴趣有所增加。已引入新材料和方法将这些修复体粘结到树脂材料上。由于我们对如何优化这种粘结的了解有限,本研究的目的是检验以下假设:各种表面处理变量以及这些变量的组合对陶瓷嵌体的陶瓷/复合材料界面强度有不同影响。研究了材料成分、表面粗糙化方法、硅烷处理、硅烷热处理和储存条件对粘结强度的影响。研究了三种陶瓷(Dicor、Mirage、Vitabloc)、三种表面粗糙化方法(蚀刻、喷砂、打磨)、三种硅烷处理(γ-甲基丙烯酰氧基丙基三甲氧基硅烷[MPS]、MPS+对甲苯胺、乙烯基三氯硅烷)、两种热处理(20℃60秒、100℃60秒)以及两种储存条件(24小时干燥、在37℃水中浸泡一年)。对于108种组合中的每一种,测试了五个样本。陶瓷圆柱体根据分组进行处理,并用双固化树脂粘结到相同陶瓷材料的块体上。测定剪切粘结强度,并通过方差分析评估实验因素。结果表明,表面粗糙化方法对粘结强度的影响最大,而陶瓷的选择影响最小。在表面粗糙化方法中,蚀刻比喷砂或打磨具有更高的粘结强度值。(摘要截短至250字)