Thornton D D
Clin Chem. 1977;23(4):719-24.
The sharpness and reproducibility of the gallium melting point were studied and the melting temperature of gallium in terms of IPTS-68 was determined. Small melting-point cells designed for use with thermistors are described. Nine gallium cells including three levels of purity were used in 68 separate determinations fo the melting point. The melting point of 99.99999% pure gallium in terms of IPTS-68 is found to be 29.771(4) +/- 0.001(4) degree C; the melting range is less than 0.0005 degree C and is reproducible to +/- 0.0004 degree C.
研究了镓熔点的尖锐度和重现性,并根据国际实用温标1968(IPTS - 68)确定了镓的熔化温度。描述了设计用于与热敏电阻一起使用的小型熔点测定池。九个镓池,包括三种纯度级别,用于68次独立的熔点测定。发现99.99999%纯度的镓根据IPTS - 68的熔点为29.771(4)±0.001(4)摄氏度;熔化范围小于0.0005摄氏度,重现性为±0.0004摄氏度。