气相色谱法测定5-氟胞嘧啶：一种改进的提取方法。
Gas chromatographic determination of 5-fluorocytosine: a modified extraction method.
作者信息
Wee S H, Anhalt J P
出版信息
Antimicrob Agents Chemother. 1977 May;11(5):914-5. doi: 10.1128/AAC.11.5.914.
Abstract
A modified procedure for the gas-chromatographic determination of 5-fluorocytosine in serum is described. A more volatile solvent mixture for extraction is used to reduce sample preparation time before chromatography. Comparison of values from assay of 12 serum samples by our method and the reference method gave a correlation coefficient of 0.99.
摘要
本文描述了一种改进的气相色谱法测定血清中5-氟胞嘧啶的方法。使用一种挥发性更强的溶剂混合物进行萃取，以缩短色谱分析前的样品制备时间。用我们的方法和参考方法对12份血清样品进行测定，所得结果的相关系数为0.99。
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