Schwedt G
J Chromatogr. 1977 Sep 1;143(5):463-71.
The possibilities for a high-pressure liquid chromatographic analysis combined with automatic fluorimetric detection of the catecholamines adrenaline and noradrenaline are described. The optimal conditions are given for a fast separation by ion exchange and reversed-phase chromatography, and for the sensitive fluorimetric determination of adrenaline by the trihydroxyindole technique when a high excess of noradrenaline is present.
描述了高压液相色谱分析结合儿茶酚胺肾上腺素和去甲肾上腺素的自动荧光检测的可能性。给出了通过离子交换和反相色谱进行快速分离以及在存在大量过量去甲肾上腺素时通过三羟基吲哚技术对肾上腺素进行灵敏荧光测定的最佳条件。